GCMS analysis results, sample AE12636, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JUNO 302\12536.D vial: 17 Acq On 4 Jun 2002 12:59 am Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.07 1.09 ug/1 68510 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 74 2 5-Hexen-2-one 98 C6H10O 000109-49-9 5 3 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 5 4 Acetone 58 C3H60 000067-64-1 4 Abundance Scan 330 (8.072 min): 12536.D (-) m/z 43.00 100.00% 43

5000 59

101 * Tr| ■ T ?

83 ■ i ■ ' ■ .1 I I • ' ' > I 7.80 8.00 8.20 8.40 . 1’1 ■ ■ I ' I I ■ ■ ‘ ■ i ' ■ ' ' i m/z 59.00 47.92% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 — ——— 59 7.80 8.00 8.20 8.40 m/z 58.00 17.13% 27 . 101

miz—> 10 20 ■ ,• ।,1......... ,1 30 +49+ • • ■ • ।। > 40 50 60 I ■ ■ ■ ■ i ■ ■ ■ ■ i

70 80 83 , । • ■ i ' ■ ‘ 1 i ■ ■ ■ ■ i

90 100 110 Abundance #63205:5-Hexen-2-one 43

"' s. • ■ i ■ ■ ■ ■ i 7.80 8.00 8.20 8.40 5000

55 15 27 50 | 83 98

mlz-> 10 I 20 I 30 38+ 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- ■ ■ i ■ ■ 1 I ' 1 ' ' I 43 7.80 8.00 8.20 8.40 m/z 41.00 7.10% 5000 101 15 71 27 -------- -----i 56 I P . ■ |*< i । > j n/z—> 10 20 30 40 50 60 70 80 90 100 110

12536.D GCMS0531.M Tue Jun 04 11:51:43 2002 Page 1

NYC-WTC_000014648