GCMS analysis results for sample AE12571, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\JUNO 302\12571.D Vial: 22 Acq On 4 Jun 2002 5:55 am Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.07 1.18 ug/1 74439 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 5-Hexen-2-one 98 C6H10O 000109-49-9 9 3 Sil ane, trimethyl - 74 C3H10Si 000993-07-7 9 4 Propane, 2-methyl-2-(1-methylethoxy 116 C7H160 017348-59-3 9 Abundance - Scan 329 (8.068 min): 12571 .D (-) m/z 43.00 100.00% 43

59 5000

101 —TT1TTeTmpt 83 7.80 8.00 8.20 8.40 51 , mmmmmmH 1pmh+ ]. >.. i'i ... ।.... ।, 111. > I. ।.... ।. TTHHTTTTP m/z 59.00 53.63% miz—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 . /7 > । . A । / > । TPp i " i 59 7.80 8.00 8.20 8.40 m/z 58.00 17.88% 27 . 101 83 । r■“i mm +P , 49 | I>.1 | | |11 I ! | I I 11|>>11 |1

m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70-75 80 85 90 95 100105 Abundance #63205: 5-Hexen-2-one 43 7.80' 8.00 8.20 8.40 5000 m/z 101.05 16.80% 1 27 55 15 83 98 mA*rr38,++ 50 TTTp ‘ *1—4411—8841841814 mfz~> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #331: Silane, trimethyl- ' * i • 59 7.80 8.00 8.20 8.40 m/z 41.00 6.27% 73 5000

45

m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 7.80 8.00 8.20 8.40

12571.D GCMS0531.M Tue Jun 04 11:52:48 2002 Page 1

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