GCMS analysis results for sample AE12286, June 2002

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Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\ JUNO3 02\12286.D Vial: 9 Acq On 3 Jun 2002 5:04 pm Operator: Sample re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) . Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.07 0.75 ug/1 46973 1,4-Dichlorobenzene-d4 12.06 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pent one, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 56 2 Aceto: 58 C3H60 000067-64-1 9 3 5-He: n-2-one 98 C6H10O 000109-49-9 9 4 Mo: oline, 4-methyl - 101 C5H11NO 000109-02-4 5 Abundance Scan 330 (8.071 min): 12286.D (-) m/z 43.0.0 100.00% 43

5000 59

101 —TT 7.80 8.00 8.20 8.40 i l u > > 111 111II111r11.1n11111 83 149171 TmmmppTTHTT m/ Z 59.00 48.08% m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43 "■I ’.. 5000 59 7.80 8.00 8.20 8.40 m/z 101.05 21.34% 27 । > ■ > ■ । > 1111 > ■ 111. > 1111 > । . 111 > I . ,, |....।...h...83 49 —H +mm , 101 । .I.|..... .p.1.11.. .j.... |, m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #62326: Acetone 43 1 ' ' ' I ' 1 1 1 I' ' 1 ' 1 1 1 1 1 I ! ' ' ' 7.80 8.00 8.20 8.40 5000 m/z 58.00 20.12% 58 27 . n/z-> m pr •rr-rrrpTTTp-m-]-rrrrp-rrrp-rrr^^ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63205: 5-Hexen-2-one ■ ' ■ ■ i ‘ ■ i ■ ■ ■ ■ i 1 ■ ■ ■ i ■ • ■ • 43 7.80 8.00 8.20 8.40 m/z 41.00 8.96%

5000

27 55

m/z-> 15 11717138,1 50 83 98 'I" ''I'" 'I" ।... 11,... ।.... ।,... (.. 11111,11111 ■ 11111111111111:11 5 10 15 2025303540 45 50556065 70 75 80859095 100105 h... I HU.... 7.80 8.00 8.20 8.40

12286.D GCMS0531.M Tue Jun 04 09:03:51 2002 Page 1

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