Laboratory report documenting GCMS analysis of sample AE09447 including surrogate recovery data conducted on May 15, 2002.
NYC-WTC_000045462–000045471Folder label: “GCMS X 5/3/02 A 5/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C: \HPCHEM\1\DATA\MAY0802\9447.D Vial: 12 Acq On 8 May 2002 9:20 pm Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator). Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
8.16 15.03 ug/1 916194 1,4-Dichlorobenzene-d4 12.19
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 2 - Pentanone , 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 Acetone 58 C3H60 000067-64-1 9 3 5-Hexen-2-one 98 C6H10O 000109-49-9 7 4 Butane 58 C4H10 000106-97-8 5 Abundance Scan 341 (8.162 min): 9447.D (-) m/ z 43.00 100.00% 43
5000 59 ........ J.................... i 1 | 1 T I | । । । I | I I I-! | k 101 780 8.00 8.20 8.40 8.60 ........................... 38 1 1153I| I. I l 67l ll 83 dnn—m—n—gn.d I ff > I I [1 J m/ Z 59.10 43.90% I I I I I I < I “I I' "l ' I_ I U > I I I I
m/z-> 10 20 30 40 50 ।60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43
5000 ■ > r1 ■ 1 1 r1 1 1 ■ i ■ ■ ■ri 1 1 r ‘ i 1 59 780 8.00 8.20 8.40 8.60 m/z 58.10 17.31% 27 101 .......... +49 50 60 ■11'" I 70 | 1 1 ■ ■ i ■ ■ ' ■ i 80 83 ■' ■ 1 ' I 90 ii1"" i'1 100 110 m/z~> 10 20 30 40 Abundance #62322: Acetone 43
7 80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.64% 58 27 ■ ■ । ■ ■ ■ ■ । 1 ■ i 1 1 ■ 'I1 1 mlz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205: 5-Hexen-2-one 4)3 780 8.00 8.20 8.40 8.60 m/z 41.00 7.10%
5000
55 15 27 50 | 83 98 ........ iI r | ......... 1......... 38 I > I I ' I I I I I I I I I I I I I I II I I I I I I k I I I I 7—I i ' | ~| 'i — i 1 i I | I i T- 1 -- 1 | I 1 n 1 ' 1 ।f' । ' III III m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60
9447 .D GCMS0507.M Thu May 09 14:42:52 2002 Page 1
NYC-WTC_000045469
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NYC-WTC_000045516
Laboratory report documenting GCMS analysis of sample AE09451 including surrogate recovery data conducted on May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045480
Laboratory report documenting GCMS analysis of sample AE09448 including surrogate recovery data conducted on May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046303
Laboratory report documenting GCMS analysis of sample AE09586 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045498
Laboratory report documenting GCMS analysis of sample AE09449 including surrogate recovery data conducted on May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045443
Laboratory notes describing re-extraction and re-analysis of sample AE09391 due to initial recovery issues on May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046284
Laboratory report documenting GCMS analysis of sample AE09585 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046266
Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE09580 on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043667
Summary of GC/MS analytical results for sample AE08838 processed on May 7, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043716
Analytical report for sample AE08934 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046321
Laboratory report documenting GCMS analysis of sample AE09587 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046340
Laboratory report documenting GCMS analysis of sample AE09334 conducted on May 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015093
Laboratory report documenting GCMS analysis of sample AE12285 with surrogate recovery data and identification of unknown compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000045396
Department of Environmental Protection GCMS analysis record for the World Trade Center site dated May 3-8 2002.
Filed in the same folder
NYC-WTC_000045397
Single fragmented page from a Department of Environmental Protection record dated May 3, 2002 with illegible content.
Filed in the same folder
NYC-WTC_000045400
GCMS blank analysis report for sample AE09447 listing compounds below detection limits from May 8, 2002.
Filed in the same folder
NYC-WTC_000045411
GCMS calibration report for sample AE09447 showing recovery percentages for various compounds from May 8, 2002.
Filed in the same folder
NYC-WTC_000045415
GCMS reference standard report for sample AE09447 showing quantified compound levels from May 8, 2002.
Filed in the same folder