GCMS analysis results for sample AE09586, May 2002

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0802\9586.D Vial: 19 Acq On 9 May 2002 4:11 am Operator: Sample RE-EXT. Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.15 16.95 ug/1 1098140 1,4-Dichlorobenzene-d4 12.19

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 9 3 5-Hexen-2-one 98 C6H10O 000109-49-9 7 4 Acetone 58 C3H60 000067-64-1 7 Abundance Scan 340 (8.154 min): 9586.D (-) m/z 43.05 100.00% 43 ft 5000- 59 .......................... 101 7.80 8.00 8.20 8.40 8.60 ................................ 3? | 53 , 69 83 . | i । |’’ ’"1UUOOI । ।1 r । । । -4 I _ I ' I " l ~ l' I_ I l~> 1 I 1 I I I I I I I [ I I I 1 I I m/z 59.10 42.02% m/z--> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

- 5000 1 1 i 1 ‘ 59 7.80 8.00 8.20 8.40 8.60 m/ z 58.10 16.60% 27 101 . 49 ,,| 83 ’’’’’’I 4 .....401 T——p-m 1,........ m/z-> 10 20 30 50 60 70 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43

780 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.34%

38,4 1*/** 56 72 1 00 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205: 5-Hexen-2-one ' ' ) > 1 1 ' | 1 ' ' ' I ■' tTt ’’’I’ 43 7.80 8.00 8.20 8.40 8.60 m/z 41.15 7.02%

5000

55 15 27 50 | 83 98 I 1d1d . I-1 [ . I I I I I 384 1n iii । । ■ । । । । । i i — 1 i t । i i i I j j i । ।_ । r T i TY ' ' ■ [ । / Tgai 1P) । । 10 [ 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

9586 .D GCMS0507.M Fri May 10 08:22:41 2002 Page 1

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