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GCMS analysis results for sample AE10807, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE10807 conducted on May 17, 2002.

NYC-WTC_000046360–000046371

Folder label: “GCMS X 5/7/02 A 5/9/02”

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Scanned page image, NYC-WTC_000046367
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAY0802\10807 .D Vial: 22 Acq On 9 May 2002 7:08 am Operator: Sample GC/MS SCAN 5/7 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.16 13.89 ug/1 827177 1,4-Dichlorobenzene-d4 12.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 CH2=CHCH2C (O) OCH3 100 C5H802 003724-55-8 9 3 5-Hexen-2-one 98 C6H10O 000109-49-9 7 4 Acetone 58 C3H60 000067-64-1 7 Abundance L Scan 340 (8.158 min): 10807.D (-) m/ z 43.05 100.00% 4)3

5000 59 i । । । । । II । । 1 r ■ । । । । I j । i । । । । 101 7.80 8.00 8.20 8.40 8.60 ..................... 38 / 1153.|11/1/1.1 1 1 l ri—' ' | 69 1 1 ' ' | 1 ' 1 ' | ' 83 . | I I | | ' | I | | ~ r- I I I T ( l > 1 | I m/z 59.10 42.95% m/z-> 10 20 30 40 50 I60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 4(3

_____ ____ _ i 1 1 1 1 । ■ 5000 ' 1 i ‘ ' < । । i । 1 > । । 1 59 7.80 8.00 8.20 8.40 8.60 m/ z 58.10 16.54% 27 101 49 . 83 m/z->_____ 10 20 I,/... t30 40 50 60 70 d 80 ' ' i ' ' ' ■ i 111 1 1 i 90 1100J' , -110 — Abundance #1448: CH2=CHCH2C(O)OCH3 43 111 9 । .... । -r 7.80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.40%

■ 1 i ■ 1 1 ■ i ' ' ' ■ i T 38 — 1 7 100 i 1 ■ ■ ■ i ' 1 1 1 I 1 ' 1 1 I ' m/z->10 20 30 40 50 60 70 80 90 100 110 Abundance #63205: 5-Hexen-2-one __ 1 1 i ' ' 4)3 7.80 8.00 8.20 8.40 8.60 m/z 41.05 7.07%

5000-

27 55 15 50 | 83 98 I ...........I............ TPT • 1 । 1 1 1 1 । ■ 1 38 , ■ ' i ■'' 1 1 i 1 ' ' ' i 1 1 ' 1 I ''1 1 1 i ' ■ 1 1 i ■ 1 1 1 i 1 P[ m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

10807.D GCMS0507.M Fri May 10 08:21:06 2002 Page 1

NYC-WTC_000046367

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NYC-WTC_000046367Source: NYC Law Department, mirrored locally

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