Laboratory report documenting GCMS analysis of sample AE10159 conducted on May 10, 2002.
NYC-WTC_000044804–000044814Folder label: “GCMS X 4/29/02 A 5/3/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\MAY0602\10159.D Vial: 7 Acq On 7 May 2002 11:42 pm Operator: Sample GC/MS SCAN 4/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C : \DATABASE\NBS75K. L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
8.16 35.18 ug/1 2399760 1,4-Dichlorobenzene-d4 12.19
Hit# of 5, Tentative ID MW MolForm CAS# Qual
1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 Acetone/ 58 C3H60 000067-64-1 9 3 CH2=CHyH2C(0)OCH3 100 C5H802 003724-55-8 9 4 5-Hexen-2-one 98 C6H10O 000109-49-9 7 Abundance Scan 341 (8.163 min): 10159.D (-) m/z 43.05 100.00% 4)3
5000 59 - — 101 7.80 8.00 8.20 8.40 8.60 0 A +t 53 , TTH+ -H m/ z 59.1069 77 83 110010011272110022012717 r "' i m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 42.82% Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43
_____ — _______ 5000 _ 1 "TE ‘ i > | i i i | i i r । | i i i “f । r
59 7.80 8.00 8.20 8.40 8.60 m/ z 58.10 17.16% 101 83 49 ,, +TTT 122731 TH mH m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #62322: Acetone 43
780 1 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.96% 58 27 । m । ir+l r ii TIIHI 111"' i'1" l11 ■ । 1।' i'''; i ‘।" i' ’'' । ■1 ’ ■ i ■ ’ ■ ’ i ’"' ।'1111 m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #1448: CH2=CHCH2C(O)OCH3 ■ I I I I I I I I I i l ] III I T‘ 1“I I 1“
43 7 80 8.00 8.20 8.40 8.60 m/z 41.05 6.94%
5000
58 i11111 —34+ 1 72 1TTTTTTTTTTTTTTTTTTTTPTTTTTOPT1PTTTPPPOTTTTIT11I 100 J • 11 I ) I j l I / 1 I I TP I I I I I I I
m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 7.80 8.00 8.20 8.40 8.60
10159.D GCMS0507.M Thu May 09 11:12:12 2002 Page 1
NYC-WTC_00004481 1
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NYC-WTC_000044836
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10165 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045423
GCMS analytical report for sample AE10607 showing unknown compounds and surrogate recovery data from May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044815
Laboratory report documenting GCMS analysis of sample AE10161 conducted on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044349
Laboratory report documenting GCMS analysis of sample AE09565 conducted on May 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044338
Laboratory comment noting low recovery in initial GCMS scan of sample AE08264, resulting in re-extraction.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045386
GCMS analytical report for sample AE10522 showing unknown compounds and surrogate recovery data from May 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043291
GCMS results for sample AE09521 showing surrogate recovery and unknown compounds dated May 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045353
GCMS analytical report for sample AE10519 focusing on unknown compounds from May 21, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043310
GCMS results for sample AE09524 showing surrogate recovery and unknown compounds dated May 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045247
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10434 conducted on May 20, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023316
Laboratory report showing GC/MS analysis results for sample AE09578 including surrogate recovery data on May 16, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014700
Laboratory report documenting GCMS analysis of sample AE12572 conducted on June 7, 2002, including surrogate recovery data.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044378
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 29 and May 3, 2002.
Filed in the same folder
NYC-WTC_000044379
Fragment of a document containing unreadable text and partial headers from a DEP laboratory procedure.
Filed in the same folder
NYC-WTC_000044381
Gas chromatography-mass spectrometry blank analysis showing results below method detection limits for organic compounds.
Filed in the same folder
NYC-WTC_000044396
Calibration data for GCMS analysis of volatile organic compounds recorded on May 7, 2002.
Filed in the same folder
NYC-WTC_000044397
Calibration data for GCMS analysis of volatile organic compounds recorded on May 6, 2002.
Filed in the same folder