GCMS analysis report for sample AE09523, May 2002

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAY0202\9523 .D Vial: 21 Acq On 3 May 2002 10:38 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.17 10.49 ug/1 580154 1,4-Dichlorobenzene-d4 12.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 CH2=CHvH2C(0)OCH3 100 C5H802 003724-55-8 9 3 Acetone 58 C3H60 000067-64-1 7 4 5-Hexen-2-one 98 C6H10O 000109-49-9 7 Abundance Scan 342 (8.173 min): 9523.D (-) m/z 43.05 100.00% 43 A

5000 59 ___ ______ ____ _______ । । । । । t-] । III l । । । । । । । k i- 101 780 8.00 8.20 8.40 8.60 ............................... t 3? । 53 , 83 . ! I l I I I J-1 I I I I I I I ' ( ' I I Ii । । 7 ■ r 1 — I I I 1 | I | | i | Th i I | I I I I p I i I | I m/z 59.10 41.42% m/z--> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 , । । . 59 7.80 8.00 8.20 8.40 8.60 m/ z 58.10 16.89% 27 101 i....... n...I,/..... r +49+ 83 1 1 ■ • 1 i 1 1 ■ 1 i 1'1 1 ' i । । ■ ■ ■ ■ । ■

m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 7.80 8.00 8.20 8.40 8.60 5000 m/Z 101.15 12.72%

58 72 100 38 n - ' i ■ ■ 1 1 i ' 1 1 1 I ' 1 1 1 i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #94: Acetone 43 7.80 8.00 8.20 8.40 8.60 m/ z 41.05 6.86%

5000 15 58 27 i । । i'll । । ।.. ,17, । । । —4 1 1 i 1 ' i 1 ' ' 1 1 1 1 1 1 1 1 1 • ' I 1 1 1 1 1 11 1 ' 1 1 1 । 1 1 I TI I i I I I | I I t j ) । T I । I

m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

9523.D GCMS0501.M Fri May 03 12:24:12 2002 Page 1

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