GCMS analysis results for sample AE10807, May 2002

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Laboratory report documenting GCMS analysis of sample AE10807 conducted on May 17, 2002.

NYC-WTC_000046360–000046371

Folder label: “GCMS X 5/7/02 A 5/9/02”

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Data File C:\HPCHEM\l\DATA\MAY0802\10807.D Vial: 22 Acq On 9 May 2002 7:08 am Operator: Sample GC/MS SCAN 5/7 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.79 2.17 ug/1 161941 Naphthalene-d8 15.83

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopent a ail oxane, decamethyl- 370 C10H3005Si5 000541-02-6 2 Benzeneet namine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 3 3,4-Dihyd oxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38 4 Benzeneethanamine, N- [ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 37 Abundance Scan 1064 (14.793 min): 10807.D (-) m/z 73.10 100.00% 73

5000 267 355 ........ /.......... I | 1 II 111 t fl I I I I I I I I 1 1_ I 1 I

45 14.40 14.60 14.80 15.00 15.20 125154 193 237tin. । । 323 i i । ) i i '। J" n "I -I | 1 (' i ) M । 'i i 1111’71 •"‘1 1 1 1 ‘ ‘ ‘ m/z 267.05 32.75% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 । । । । — । i । i r — ■ । i । i i i i । i r 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 30.57% 1** 207 323, ‘ ‘I m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 ■ । ■ ■ ■ । t ■ ■ 7 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.10 10.81%

45 | | 208 251 281 , 386 458 548 TI——————TTIT I1/1/4/***/‘I1I*II**I1‘* miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 14.40 14.60 14.80 15.00 15.20 m/ Z 74.10 8.60% 267 5000 179 356 45 147 209 237, 312 01 1 1 1 1 1 1 ' i' 1 1 1 i r 1 r 1 i 1 1 ' ■ i 1 1 1 1 1 1 1 I | I I I I | i | I r A I i i । i i i i । i r

m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20

10807.D GCMS0507.M Fri May 10 08:21:08 2002 Page 2

NYC-WTC_000046368

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