GCMS calibration table data, May 2002

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Calibration table data for GCMS analysis of volatile organic compounds dated May 3-6, 2002.

NYC-WTC_000046249–000046265

Folder label: “GCMS X 5/7/02 A 5/9/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY0302\9579.D Vial : 9 Acq On 3 May 2002 9:52 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Cyclopentasiloxane, decamethyl Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 14.79 1.74 ug/1 134660 Naphthalene-d8 15.83 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6(80 2 3,4 -Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 49 3 N-(Trifluoroacetyl)-0,O011-tris(t 481 C19H34F3NO4Si3 000000-00-0 47 4 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 47 Abundance l Scan 1064 (14.791 min): 9579.D (-) m/z 73.10 100.00% 73

5000 267 355 ......... _ 1 i 1 1 1 ' i । । 1 • i ■ ' 11 I' ■'

45 14.40 14.60 14.80 15.00 15.20 I i 108 133154 193 223 , 323 [ 1 1 l 1 ’ ' ' i ' ' ' ' I 1 ' 1 1 i ' 1 ' 1 i ' m/z 267.05 30.81% m/z->______ 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 5000 267 TI TT A 1 i 1 1 14.40 14.60 14.80 15.00 15.20 m/z 355.10 27.11% 207 323 '' 1 ' i 1 1 ■ ' i 1 1 1 ■ i r m/z-> 50 100 150 200 250 300 350 400 450 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 i | i i i i — i i r P i i i । — i I । i r

14.40 14.60 14.80 15.00 15.20 267 m/z 356.10 10.21%| 5000 179 356 45 147

1 1 i ......... I, 1 ' l ' ' ' ‘ i 1 ‘ ' 209 237 , I ' 1 1 1 i 1 r 312 . , । । । r । > । । < [■■ । । ■ । ।“| i m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-tris(trimethylsilyl)no TT Tkr 73 14.40 14.60 14.80 15.00 15.20 m/ Z 74.10 8.25% 355 5000

45 TU 1 L 1 ___ “126147 1 I । । । t t T T 11 i ' 193 । । । । 265 j "। i T i i । । । “r 376........ 481 m/z—> 50 100 150 200 250 300 350 400 450 | 14.40 14.60 14.80 15.00 15.20

9579 .D GCMS0501.M Mon May 06 10:49:54 2002 Page 7

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