GCMS calibration table data, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0302\9579.D Vial: 9 Acq On 3 May 2002 9:52 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 Nonanoic acid Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 16.99 0.50 ug/1 38405 Naphthalene-d8 15.83 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Nonanoic acid 158 C9H18O2 000112-05-0 59 2 Octanoic/Acid 144 C8H16O2 000124-07-2 50 3 Hexanoi acid 116 C6H12O2 000142-62-1 40 4 Octangic acid, silver(1+) salt 251 C8H16AgO2 024927-67-1 37 Abundance 7 Scan 1304(16.991 min): 9579.D (-) m/z 60.00 100.00% 60 73 A 5000 41

TT LA A I I ’ I I I I I I I I I I I — 115 129 ...... ........................................................... 16.60 16.80 17.00 17.20 17.40 -H+ W i i i । i i i i । n i i J i i i I j n । । । । i i । । । । i i । । । i > J i n i | । > m/z 73.10 78.75%

L m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #11977: Nonanoic acid 63 73

5000 TT ‘ I ' 1 1 ' I ELT 27 16.60 16.80 17.00 17.20 17.40 115 m/ z 57.10 63.41% 87 98 129 l 'I 1 I " 'I' 1 " '‘I I1 158 T’Il ' I TTIT T1 l i t | I I-1 i | i r

m/z-> 20 30 40 50 60 70: 80 90 100 110 120 130 140 150 160 Abundance #66327: Octanoic Acid 63 ’F A AH TL" I Ttl

C 73 1660 16.80 17.00 17.20 17.40 5000 m/z 41.10 48.07% 45 85 101 ' r ■ 1 1 i 1 1 1 ■ i Ili I 115 | 1l’111111/1/1/1/1/1/1/1/-*11, ’IT 129 144 ——//—/OOTCB/—nIB/CT/B/T/T/t/tr/1/k, m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #3243: Hexanoic acid । । । I । । । । । । । । । i । । । i । i i । i r I 60 16.60 16.80 17.00 17.20 17.40 m/ Z 43.05 43.81% 5000- 73 27

m/z-> 20 30 — 40 45

50 60 TrI 70 80 87 ‘ ' i 1 90 101 T-p-r 100 110 120 130 140 150 160 AAAonan) 1 l I t I I ’ 11 I

16.60 16.80 17.00 17.20 17.40 I I I I I I (I I TT"u

9579 .D GCMS0501.M Mon May 06 10:49:55 2002 Page 8

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