GCMS analysis comments for sample AD28663, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC0401\28663.D vial: 17 Acq On : 5 Dec 2001 3:59 am Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise t Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Nonacosane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 36.28 0.41 ug/1 63591 Perylene-dl2 37.13 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Nonacosane 408 C29H60 000630-03-5 2 Hexatriacontane 507 C36H74 000630-06-8 86 3 Heneicosane 296 C21H44 000629-94-7 83 4 Nonadecane ___________________ 268 C19H40 000629-92-5 83 Abundance Scan 3403 (36.281 min): 28663.D (-) m/z 57.00 100.00% 57

85 5000

....................... .. ................................ 36.00 36.20 36.40 36.60 m/z 71.10 69.96% m/z-> 40 60 80 100 120140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #54526: Nonacosane 43

71 5000 1 AAA,YY 1 ■ —4 A ।, 4 36.00 36.20 36.40 36.60 m/z 43.00 65.14% i 99 | | tf ,127,________ 211 239________________ 379 408 IT —C—00"T0—1—E"1I—u——""——OU“gu"I"I“O‘I"u"u—nueri ‘ ‘‘ mz-> 40 60 80 100120140160180 200 220 240 260 280 300320 340 360 380 400 Abundance #74635: Hexatriacontane 57

‘36.00 36.20 36.4036.60 3 5000 85 m/z 85.05 57.84%

n/z-> — 4 .......... .. . 40 60 80 100 120 140 160180 200 220 240 260 280 300320 340 360 380 400 ' Abundance #42201: Heneicosane ------- -MA -- —i 57 36,00 36.20 36,40 36.60 m/z 55.00 25.96% 85 5000

m/z—> |i —1141, ‘ ‘1‘‘10011007E0 113 ... 268 296_______________ 00T0—0101010—010—00"—U0UU0000"000U0"E 40 60 80 100120140160180 200 220 240 260 280300320 340 360 380400 IMAAAAanil MeMdn 36.00 36.20 36.40 36.60

28663.D GCMS1126.M Thu Dec 06 15:31:44 2001 Page 11

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