GCMS analysis summary, sample AD31377, Feb 2002

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Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\JAN1 502\31377.D Vial: 23 Acq On : 16 Jan 2002 8:28 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Nonacosane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

34.34 0.54 ug/1 73299 Chrysene-dl2 32.79

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Nonacosane 408 C29H60 . 000630-03-5 90 2 Nonadecane 268 C19H40 000629-92-5 90 3 Triacontane 422 C30H62 000638-68-6 90 4 Tetratetracontane 619 C44H90 007098-22-8 90 Abundance Scan 3191 (34.335 min): 31377.D (-) m/z 57.00 1 00.00% 57

85 5000

A , AA 1 ft/, Mmmme,

_X 113 155 207 34.00 34.20 34.40 34.60 — I • I “ ‘ \ l • •«• I ‘ t • * l« “»I ‘ !■..>i....p.j I... । m/z 43.05 76.80% miz-2 40 60 80 100 120140 160 180200 220240 260280300 320340 360 380400420 Abundance #54526: Nonacosane 43

71 5000 AAY444—AYM 34.00 34.20 34.40 34.60 | m/ z 71.10 74.02% 99 , 127 211 239 P—u TrrrrYTTTTpTTTTTTrTpTTrpnT-rTTTTTp-rrrpn-TTpT^^ 13111111 T—BB"33TT 379 408 m/z-> 40 60 80 100 120140 160180 200 220240 260280 300 320 340 360380400420 Abundance #37483. Nongcenie 57 -A s 5000 85 I 34.00 34.20 34.40 34.60 m/z X 51.83 113 183 268 m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #55461: Triacontane -A I t . II ( | I I / I I AI I I |

43 34.00 34.20 34.40 34.60 m/z 41.05 32.07? 71 5000

m/z-> 99 I ,1 1- 127 239 267 40 60 80 100 120140 160180 200 220 240 260 280 300 320 340 360 380 400 420 379 422 MArMnlrn 34.00 34.20 34.40 34.60

31377.D GCMS1126.M Mon Feb 04 15:08:08 2002 Page 3

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