GCMS calibration data for method 508, April 23 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR2202\8757.D Vial : 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Nonanal Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

14.04 0.51 ug/1 86049 Naphthalene-d8 15.84

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Nonanal 142 C9H180 000124-19-6 45 2 Cycloheptane 98 C7H14 000291-64-5 35 3 Nonanol 144 C9H20O 028473-21-4 25 4 1-Hexanol , 3-methyl- 116 C7H160 013231-81-7 22 Abundance Scan 980 (14.040 min): 8757.D (-) m/z 57.00 100.00% 41 57 fl 5000 70 98 82 . -A 819 TTIPT I 13.80 14.00 14.20 14.40 | 1-11 1 77 I 109114 m/z 41.00 84.99% 1 i ‘ ■ 1 1 i 1 1 1 • । ■ TI 1 1 I 1 1 ■ I I I 1 I I I I II [ T m/z->___ 20 30 40 50 60 70 80 90 100 110 120 Abundance #66170: Nonanal 57

44 5000 27 M , /, sr nijoi 13.80 14.00 14.20 14.40 70 98 m/z 43.00 61.77% 82 114 1 I I I I < I ~ l— I 1 I [ Hi 1 i 1 ‘ 1 1 1 । ■ ■ ■ 1 । 1 ■ ‘ ' । 1 m/z->20 30 40 50 60 80 70 90 100 110 120 Abundance #63231: Cycloheptane 41 70 27 98 13.80 14.00 14.20 14.40 5000 m/ Z 43.9.5 57.81% 83

-4 m/z->20 30 40 50 60 70 80 90 100 110 120 Abundance #66361: Nonanol 41 56 13.80 14.00 14.20 14.40 m/z 56.00 56.26% 31 70 ft 5000 83 98

— ■ ■ । I I ■ ■ i ■ ■ MA ................................ ■ i ' 1 1 ■ I ' 1 1 ' I 1 1 1 1 ' 1 1 1 ' I 1 1 ' 1 1 ' 1 1 ' 1 1 m/z—> 20 30 40 50 60 70 80 90 100 110 120 13.80 14.00 14.20 14.40

8757.D GCMS0412.M Tue Apr 23 08:22:55 2002 Page 3

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