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GCMS blank analysis results, April 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS blank analysis for volatile organic compounds on April 2, 2002.

NYC-WTC_000058591–000058599

Folder label: “GCMS X 3/6/02 A 3/30/02

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Scanned page image, NYC-WTC_000058597
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\LB.D Vial: 4 Acq On : 29 Mar 2002 5:55 pm Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyciopentasiioxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.85 0.42 ug/1 58557 Naphthalene-d8 15.88

Hit# of 5 Tentative ID MW MolForm '' CAS# Qual ------------------------ 1 Cyciopentasiioxane, decamethyl- 370 C10H3005Si5 000541-02-6 59 2 N-(Trifluorbacetyl)-N,0,0',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 47 3 PhenethylaMine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 4 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 Abundance .......................... .. Scan“l068 (14.&46 rnin)?LB7D“(-) m/z 73.00 100.00%' 713

5000 267 355

45 125 154 193 237 14.60 14.80 15.00 15.20 I I .^25 ' ' I ' m/z 267.00 45.70% rn/z-;> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyciopentasiioxane, decamethyi- 73 I I 5000 267 355 I n 14.60 14.80 1^ 15.20 ( m/z 355.05 44.31% 323 1 m/Z“>- 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifloo'-oacetyl)-Nb,O’.O"-tctrakis(tri.'-!iethylsi 73

355' 14.60 14.80 15.00 15.20 5000 m/z 356.OS 15.64%

45 147 193 257 i 538 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74239; Phenethylamine, N-methyl-.beta.,3,4-iris(trimethyls I 7)3 14.60 14.80 15.00 15.20 i i m/z 267.9,0 12.78% 5000 355 44

m/z-> J.50 100 147 150 193 200 250 267 294 300 350 400 450 500 550 14.60 14.80 15.00 15 20

LB.D GCMS0308.M Tue Apr 02 11:11:28 2002 Page 1

NYC-WTC_000058597

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NYC-WTC_000058597Source: NYC Law Department, mirrored locally

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