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GCMS analysis results for sample AE05746, April 11 2002

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Laboratory report documenting GCMS analysis of sample AE05746 conducted on April 11, 2002, including surrogate recovery data.

NYC-WTC_000059565–000059575

Folder label: “GCMS X 3/12/02 A 4/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APRO102\5747.D Vial: 26 Acq On 3 Apr 2002 1:59 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

14.85 0.31 ug/1 59595 Naphthalene-d8 15.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopenta^l oxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Phenethylline, N-methyl- .beta. , 3,4 399 C18H37NO3Si3 010538-85-9 38 3 N-(TrifWoroacetyl) -0,0',0' '-tris (t 481. C19H34F3NO4Si3 000000-00-0 38 4 Noradr^aline, tetra-TMS 4 57 C2 0H4 3NO3Si4 000000-00-0 37 Abundairce. ........ ............ . ...... . Scan' 1068 (14;846 rnin): 5747□■(-) m/ z 737dy. iooTm 7l3

5000 267 355 l\ 45 14.60 14.80 15.00 15.20 i 125 154 191 223 , ' I ' ''' ■ i' r ■ 11' I "i 1' I -1 f I 1 I 323 , [ m/z 267.00 47.89% 50 100 150 200 250 :300 350 400 450 Abundance #51266: Cyclopentasiloxane, decarnethyl- 73

355 I 5000 267 AU 14.60 14.80 15.00 15.20 1

I m/z 355.0.5 46.00% I 207 323 I 50 100 150 200 250 300 350 400 450 Abundance #<4239; Phenethylamine. N-rne:hyt-.&cta..3.4-tris{triiTiethyls I 7i3

14.60 14.80 15.00 15.20 5000 355 m/z 356.05 15.86% 44 147 193 267 294 rn/zj^;50 100 150 200 250 300 350 400 450 Abundance #58326: N-(Trifluoroacetyi)/b,b',d"-tris(trimethyisilyf)no i 7|3 14.60 14.80 15.00 15.20 355 m/z 267.90 13.27% 5000

45 I 126147 193 265 ,376........ 481 im/z~> 50 100 150 200 250 300 350 400 450 14.60 14.80 15.00 15.20

5747.D GCMS0403.M Fri Apr 05 10:39:43 2002 Page 3

NYC-WTC_000059574

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NYC-WTC_000059574Source: NYC Law Department, mirrored locally

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