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GCMS analysis results for sample AE05746, April 11 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05746 conducted on April 11, 2002, including surrogate recovery data.

NYC-WTC_000059565–000059575

Folder label: “GCMS X 3/12/02 A 4/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR0102\5747.D Vial: 26 Acq On 3 Apr 2002 1:59 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★ Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.28 0.38 ug/1 55194 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanon^, 1,1,1-trichloro- 160 C3H3C13O 000918-00-3 40 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 5 3 Glycine,7^-acetyl- 117 C4H7NO3 000543-24-8 4 4 2-Propaffone, 1,1-dichloro­ 126 C3H4C12O___ _ 000513-88-2 4 Abundance..........S«in353(a283ni^^ 4(3 m/z 42.95 Too'. oo%i

5000

10 20 30 40 ,49 50 60 63 70 93

.8Q._..9O 100 97

110 120 130 8.00 m/z 124.85 u, 8.20 8.40 8.60 9.49% Abundance 2-Propanone, 1,1 J-trichioi^ 4b

5000 .................... .................... 8.00 8.20 8.40 8.60 __ ! 15 m/z 82.85 6.98% 35 ,49 85 97 117 125 m/z->10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4 / 32 ■ N-Acetyipyrrolidonc 43

8.00 8.20__ 8.40 8.60 5000 m/z 126.90 6.86% 99 127 56 86 39 69 I . 112 i -r-ryT-T-T-Tq-T-T-T-T-j^^ 'm/z-> 10 20 30 40 50 60 70 80__ 90 100 110 120 130 Abundance #3394: Glycine, N-acetyT- ........ 3l0 8.00 8.20 8.40 8.60 43 m/z 81.85 6.06% 5000 72 15 I J 56 ■Y, I , ,I,I , I....... ...... ......... 10 20 30 40 50 60 70 80 90 100 110 120 130 8.00 8.20 8.40 8.60

5747.D GCMS0403.M Fri Apr 05 10:39:39 2002 Page 2

NYC-WTC_000059573

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NYC-WTC_000059573Source: NYC Law Department, mirrored locally

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