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GCMS analysis results for sample AE05745, April 11 2002

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Laboratory report documenting GCMS analysis of sample AE05745 conducted on April 11, 2002, including surrogate recovery data.

NYC-WTC_000059555–000059564

Folder label: “GCMS X 3/12/02 A 4/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR0102\5746.D Vial: 25 Acq On 3 Apr 2002 12:59 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00’ MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* . Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.28 0.30 ug/1 41514 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propan^e, 1,1,1-trichloro- 160 C3H3C13O 000918-00-3 64 2 4-Pente^2-one 84 C5H8O 013891-87-7 9 3 1-Fluo^nonane 146 C9H19F 000463-18-3 9 4 1-Oct^ecanol 270 C18H38O.... 000112-92-5 9 Abundance ' Scan 353 (8.282 min); 5746.D (-) ' m/ z 43?^. iob?^ i 4i3

'm/z->10 5000

20 .... 30 40 1^9 50 60 63 74 62 ' I " ' ' I I'l' 70 80 97 90 100 I,

110 120 130 8.00 m/z 124.8 K 8.20 8.40 8,60 8.35% Abundance » #12247: 2-Propanone, 1,1,1-trichloro- i 43 I I 5000 8.00 8.20 8.40 8.60___ 15 m/z 7,. 69% ! 35 i ,49 85 97 117 125 I ' I I ' ' ' I ' ' I ' ' ' ' I ' ' ' * I ' ' ' ■ I ' ' ' ' I ' ' ' ' I ' ' ' m/z->____ 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #555' 4-Pcnteri-2-one 43

____ 8.00 8.20 8.40__ 8.60____ 5000 m/z 126.90 ' 7”‘. 69%

15 ! ¥ 37. .53 69 84 , ,____ ' 10I ' ' ' ‘20I ' ' ‘ '30I ' ' ' '40I ' ' ' '50I ' ' ' '60I ' ' ' '70I ' ' ' '80I ' ' ' '90I ' ' ' 100 Ifp/Z;;> ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 110 120 130 Abundance #8922; 1-Fluorononane . . ...... J............. 4|3 8.00 8.20 8.40 8.60 I m/z 81.95 7.00% 5000 56. 27 70 84 97 33 I I h 10 20 30 40 50 60 70 80 90 100 110 120 130 8.00 8.20 8.40 8.60

5746.D GCMS0403.M Fri Apr 05 10:38:40 2002 Page 2

NYC-WTC_000059563

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NYC-WTC_000059563Source: NYC Law Department, mirrored locally

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