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GCMS analysis results for sample AE05703, April 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05703 conducted on April 11, 2002, including surrogate recovery data.

NYC-WTC_000059526–000059535

Folder label: “GCMS X 3/12/02 A 4/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR0102\5743.D Vial: 22 Acq On 2 Apr 2002 10:00 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.28 0.32 ug/1 49329 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 , Tentative ID MW MolForm CAS# Qual

1 2 - Propano/ne, 1,1,1-trichloro- 160 C3H3C13O 000918-00-3 56 2 Ethanol ,/2,2,2-trichloro- 148 C2H3C13O 000115-20-8 9 3 2-Propione, 1,1-dichloro- 126 C3H4C12O 000513-88-2 9 4 Decan^ 1-fluoro- 160 C10H21F _000334-56-5 9 Abundance....... ( .... Scan 353(8583miin^'^^ m/ z 43 ?05 100?^% ' 43 i

1 5000

35 l| I p r I I I I I r I I I I'I'i I I

/n/z->10.. 20.... 30 40 ,151 61 71 Jg.. ?, 50 60 70__ 80__ 90 ’if 100.110 120 130 140 J 50 . t I . I JUu 8.00 m/z 124.85 8.20 8.40 8.60 • 11.07% Abundance #12247: 2-Propanone, 1,1,1-trichloro- 40

5000 8.00 8.20 8.40 8.60 15 m/ z 82.85 9.17% I 111''' p 35 : 97 117 125 ' I ' ' ' 11 ■ p'' ''I'l. ' I ' ' ' ' I ' ' ' ‘ I ' ' I ' I ' ' ' ' 1 ' ' I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #60531. Ethanol, 2,2,2-trichloro- 31

8.00 8.20 8.40 8.60 5000 m/ z 96.95 7.91% 49 77 84 113 I 61 i 150 I ”^1“* '

__ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #4368: 2-Propanone, 1,i-dichloro- ............ 4j3 ;___100_8;2g_840_jBJ6^^ m/z 126.90 7.60% 5000

15 im/z-> I ' I ' ' ' ' I ' ‘ ' I ' ' ' ’ , ,■!... . . , .7^. ..................... 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 J 8.00 8.20 8.40 8.60

5743.D GCMS0403.M Fri Apr 05 10:36:24 2002 Page 2

NYC-WTC_000059534

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NYC-WTC_000059534Source: NYC Law Department, mirrored locally

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