GCMS unknown compound analysis, sample AE05516, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR0102\5516.D Vial: 7 Acq On 1 Apr 2002 6:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L **************************************.******************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstCone Area Relative to ISTD R.T.

8.28 0.46 ug/1 70691 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Z Tentative ID MW MolForm CAS# Qual

1 2-Propan®ne, 1,1,1-trichloro- 160 C3H3C13O 000918-00-3 38 2 2-Pente^, 2-methoxy- 100 C6H12O 061142-47-0 9 3 Ethanol/ 2,2,2 -trichloro- 148 C2H3C13O 000115-20-8 9 4 2-Pent/nethiol 104 C5H12S 002084-19-7 7 Abundance Scan 352 (8.280 min): 5516.D (-) m/ z 43

5000

35 83 97 8.00 8.20 8.40 8.60 ' I ' ' ' ‘ I '' '' I ' 11 . ............... '.'I r-rq-T-rrr I I I . . I i ... I m/z 124.8,5 10.54% 'm/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 ......................... 8.00 8.20 8.40 8.60

15 m/z 96.95 7.81% I 35 97 117 80 '' ' I ' '' ' I ' ' '' ■p-r-r-rj-m-r-p m/z-> 10 20 30 40 50 M 70 90 100 110 120 130 140 150 'Abundance #1570: 2-Pentene, 2-methoxy- ^3 55 72 . 85 i .... II.... ___Jk00__J;20__8A0^^ 5000 100 m/z 46.95 7.67% I

I , J -J;, '{ J . I I ni/z->____ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66531: EthanoI72X2-M^^ 1 8.00 8.20 8.40 8.60 m/z 82.85. 6.27% 5000 49 77 113 61 1111 . 150 nn/z--> 10 20 30 40 50 60 70 80 90 100 110. 120 130 140 150 8.00 8.20 8.40 8.60

5516.D GCMS0403.M Thu Apr 04 13:54:19 2002 Page 2

■ NYC-WTC_0b0059294 '