GCMS analysis results for sample AE12678, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\l\DATA\JUN0302\12678.D Vial: 10 Acq On 3 Jun 2002 6:03 pm Operator: Sample gc/ms scan 5/31 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Propanone, 1,1,1-trichloro- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

8.11 1.09 ug/1 76437 1,4-Dichlorobenzene -d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 23 2 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 9 3 1 - F luorononane 146 C9H19F 000463-18-3 9 4 2-Acetyl/l,4,5,6-tetrahydropyridine 125 C7H11NO 000000-00-0 4 Abundance Scan 334 (8.112 min): 12678.D (-) m/z 42.90 100.00% 43

5000

11———/ ■ ■ i ' rn-p-. Pi" 97 125 7.80 8.00 8.20 8.40 36 — 49.61... 33, I, ■ i ■ ■ ■ ■ 1* ’ I’’’I ii. • i * • ■ ■ i 1E !:। ■ < > . । i * m/z 124.85 12.25 niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

5000 ' ■ ■ i ■ ■ ' ■ i ■ ' • 1 i ■ ■ ‘ ■ i ■ ‘ ■ t 7.80 8.00 8.20 8.40 m/z 96.90 8.25% 15 35 49 85 97 117 125 11 ■ i ■ ■ ’ I ’’*+1’* '11 ■ ’’4 । ■ ■ 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4368:2-Propanone, 1,1-dichloro- 43 ■ ■ • i ■ ■ ■ 1 i ‘ ( ■ i ■ • ■ ■ i ■ ■ ■ ‘ i 7.80 8.00 8.20 8.40 5000 m/z 126.85 8.12?

15 27 . J 49 63 76 83 93 37 THTTdmunuOuuTTTTDT miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 - Abundance #8922:1-Fluorononane 43 7.80 8.00 8.20 8.40 | m/z 82.95 6.63% 5000 56 27 70 84 97 33 I ■ ' i ‘ ‘ ' i 1 1 1 1 I''' 1 ' I ' ' i ■ ■ ■ 11 ■ ■ ■ • i1 ■ ■ ‘ i ' ■ ■ ■ i ■1 ■ ■ i ■ ■ ‘ 14 /z—> 10 20 30 40 50 60 ' • 70 80 90 100 110 120 130 7.80 8.00 8.20 8.40

12678.D GCMS0531.M Tue Jun 04 09:04:03 2002 Page 1

NYC-WTC_000015109