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GCMS analysis results for sample AE12678, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE12286 with surrogate recovery data and identification of unknown compounds.

NYC-WTC_000015102–000015111

Folder label: “GCMS X 5/31/02 A 6/3/02

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Scanned page image, NYC-WTC_000015110
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NYC 9/11 Public Portal Document ’ Library Search Compound Report Data File C:\HPCHEM\1\DATA\JUNO302\12678.D Vial: 10 Acq On 3 Jun 2002 6:03 pm Operator: Sample gc/ms scan 5/31 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) , . Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 25.56 0.41 ug/1 39415 Phenanthrene-dl0 25.43 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene/diO- / / 188 C14D10 001719-06-8 72 2 Phenanthrene-d10y / 188 C14D10 001517-22-2 72 3 Phosphonic acid, (3-methyl-3-pent en 188 C8H13O3P 022152-34-7 40 4 -(4-Tolyp-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 37 Abundance 7 Scan 2235 (25.564 min): 12678.0 (-) m/z 188.10 100.00%! 188

5000

80 94 158 । 25.20 25.40 25.60 25.80

miz-> ............. — - mm — 49 66 4ilaaaat*a**yesa*aa1a14 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 94.00 22.68% Abundance #19957: Anthracene-d10- 118

5000 P I ■ 1 1 ‘ I ■ * ■ ■ i • 2520 25.40 25.60 25.80 m/z 80.00 20.64%

miz-> tes. " i “ “ I ‘“ i “ “ i' 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 160 asi) rll11 Abundance #19958: Phenanthrene-d10 118 —0 25.20 25.40 25.60 25.80 5000 m/z 189.10 18.52

66 66 80 94 160 ---- - miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19736: Phosphonic acid, (3-methyl-3-penten-1-ynyI)-, dimet • 1 i ■ ■ ■ ■ i ■ 118 25,20 25.40 25.60 25.80 m/z 184.05 15.79

5000 77 62 35 47 93 109 155 TTp- miz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.20 25.40 25.60 25.80 ‘ ‘ ‘ '

12678.D GCMS0531.M Tue Jun 04 09:04:04 2002 Page 2

NYC-WTC_000015110

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NYC-WTC_000015110Source: NYC Law Department, mirrored locally

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