GCMS surrogate recovery results, sample AE01143, March 4, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\1143.D Vial: 65 Acq On : 24 Feb 2002 8:04 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.87 0.21 ug/1 17609 Phenanthrene- dl 0 25.74

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d 2 Phenanthrene-d10— ’ Z=760 188 188 C14D10 C14D10 001719-06-8 87 001517-22-2 86 3 Phosphonic/acid, (3-methyl-3-penten 188 C8H13O3P 022152-34-7 50 _4 Benzaldehyde, 2,6-difluoro-4-hydrox 188 C8H6F2O3 000000-00-0 38 Abundance / Scan 2269 (25.873 min): 1143.D(-) T m/z 18 .10 100.00% 188

5000

80 92 158 49 I| • ■ I > । । | “ 11 11 n 111 । 11 । 11 111 i ! i ■ । i i n । > I I '| i r 25.60 25.80 26.00 26.20 ’1-0-11—-311I —231103118 m/ z .95 16.69% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: AnthraceneJlO- 188

- 5000 25.60 25.80 26.00 26.20 m/z 92.00 16.57% 66 80 94 160 hl mmmmmmmmmhmmmmmmmmmmmmmPHP m/z->___ 30 40.50 60 7080 90 100 110 120130140 150 160 170 180 190 Abundance 6 ronpken* * 188 ‘ ‘ TTnnmmmm 25.60 25.80 26.00 26.20 5000 m/z 189.00 15.94%

160 66 80 94 mmmpmmpmmpmmpmppr ' ‘ 1 “ " i ■ ‘■ i ■ • “ i “ “ i ■ m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19736: Phosphonic acid, (3-methyl-3-penten-1-ynyl)-. dimet 188 25.60 25.80 26.00 26.20 m/ z 94.00 14.38% 5000 77 62 35 47 93 109 155 TTD———nuu—u]—mmmWTpo T’T - " I “ ' ‘ I' 1 “ I ‘ ‘I ■ ■ i ■1 miz—> 30 40 50 60 70 80 90 J OO 110 120 130 140150 160 170 180 190 25.60 25.80 26.00 26.20

1143.D GCMS0208.M Fri Mar 01 09:07:12 2002 Page 3

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