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GCMS analysis results for sample AE12539, June 2002

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Laboratory report documenting GCMS analysis of sample AE12539 conducted on June 7, 2002, including surrogate recovery data.

NYC-WTC_000014670–000014679

Folder label: “GCMS X 5/28/02 A 6/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\ JUNO302\12539.D Vial: 20 Acq On 4 Jun 2002 3:56 am Operator: Sample gc/ms scan 5/28 fb Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Phenanthrene-dlO Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 25.56 0.43 ug/1 38893 Phenanthrene-dl0 25.43 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene- diO 188 C14D10 001517-22-2 87 2 Anthracene -d10- 188 C14D10 001719-06-8 72 3 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 40 4 Pentacycy>[8.4.0.0(3,7) .0(4,14) .0(6 188 C14H20 000000-00-0 25 Abundance 7 Scan 2235 (25.564 min): 12539.D (-) m/z 188.10 100.00% 118

5000 94 42 66 80 158 25.20 25,40 25.60 25.80 ‘ ‘ ‘ ' —■ i “ “ i -TH — ‘ “ I 1 1' ' I " ‘' I 1 ' ‘ ' I “ “ I “ ' ‘ I' " ’Ott 11 ITI i in 11 1’H i i 11 m/z 94.00 23.99% mz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-dlO KB

5000 25.20 25,40 25.60 25.80 1 ‘'1 80 m/z 189.10 14.67% 94 160 66 miz-> 40 50 60 70 80 H I’’’ . [... 111JI J. 111111 90 100 110 120 130 140 150 160 170 180 190 -...... .............. Abundance #19957: Anthracene-d10- KB

25.20 25.40 25.60 25.80 5000 m/ z 14.36%

„ 80 94

mz-> m-rp-rTTp- 40 50 l1^....I.... ll. 60 m 70 80 90 100 110 120 130 140 150 160 170 180 190 160

Abundance #69165:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime TIT T T1" KB 25.20 25.40 25.60 25.80 m/z 184.10 14.36%

5000 143

m/z—> A40 50 60 70 80 116 130 |i 158 170 i । i । i I I > | , i i i |h . > i । I'lh i । i i i I । . ! i 41'' ' ' | ' 1 90 100 110 120 130 140 150 160 170 180 190 | I’T 1 i ■ ■ ■ I ■ 2520 25.40 25.60 25.80 IT

12539.D GCMS0531.M Tue Jun 04 11:52:21 2002 Page 2

NYC-WTC_000014678

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NYC-WTC_000014678Source: NYC Law Department, mirrored locally

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