GCMS analysis results for sample AE12539, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\JUN0302\12539.D Vial: 20 Acq On 4 Jun 2002 3:56 am Operator: Sample gc/ms scan 5/28 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) . Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.07 1.02 ug/1 66111 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4 -methyl - 116 C6H1202 000123-42-2 59 2 5-Hexen-2-one 98 C6H10O 000109-49-9 12 3 Acetone 58 C3H60 000067-64-1 9 4 3-Octanol 130 C8H180 020296-29-1 9 Abundance t Scan 329 (8,066 min): 12539.D (-) m/z 42.90 100.00%! 43

59 5000

101 7.801 8.00 8.20 8.40 .................. 38.1) +49+ 83 , | m/z !59.00 52.02 mlz-> 10 20 30 40 50 60 70 80 90 100 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 4)3

5000 59 -AP 7.80 8.00 8.20 8.40 m/z 101.05 17.82 101

miz-> ----- 10 20 27 30 40 +49 I ‘ 50 60 70 ' i 80 83 ' i ' 90 + 100 Abundance #63205:5-Hexen-2-one 4)3 ■ ■ i ■ 1 ' ■ i • 1 i ■ 1 • • i * * 7.801 8.00 8.20 8.40 | 5000 m/z !58.00 16.26%

27 55 15 83 98 iz-> | | 38,4 ■ ' i ' ■ ■ ■ i ■ ■ ■ ■ i ■ ■ 10 20 30 40 50 ' 1 i ' ■ 1 ■ i ‘ ■ 1 ■ i ■ ■ ■ 1 i ■ ■ ■ ■ i ' ■ ' 1 i ■ ■ ■ ■ i 50 60 70 80 90 100 Abundance #94: Acetone ' ■ i ■ ' ■ ■ i ’I 43 7.80 8.00 8.20 8.40 m/z 41.00 8.61% 5000 15 58

m/z—> T-TT-r 10 27 — 1 ■ TTT ■ 20 30 40 50 17,’*’I/11111,1411114 60 70 80 90 100 —AAM 7.80 8.00 8.20 8.40

12539.D GCMS0531.M Tue Jun 04 11:52:20 2002 Page 1

NYC-WTC_000014677