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GCMS analysis results for sample AE12571, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE12571 conducted on June 7, 2002, including surrogate recovery data.

NYC-WTC_000014690–000014699

Folder label: “GCMS X 5/28/02 A 6/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\JUNO 302\12571.D Vial: 22 Acq On 4 Jun 2002 5:55 am Operator: Sample gc/ms scan 5/28 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Phenanthrene-diO Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 25.57 0.40 ug/1 35522 Phenanthrene-dl0 25.43

Hit# of 5 ntative ID MW MolForm CAS# Qual ----- —- -6--- 1 Phenanthrene-diO X • 188 C14D10 001517-22-2/93 2 Anthracene-dlO- 188 C14D10 001719-06-8 72 3 Naphthalene, 2,6-dimethoxy- 188 C12H1202 005486-55-5 40 4 Antipyrine 188 C11H12N2O 000060-80-0 40 Abundance Scan 2235 (25.565 min): 12571 .D (-) m/z 188.10 100.00% 1118

5000

■ I ‘ ■ I ■ T r T '| 116* * h 4 49 66 80 94 158 25.20 25.40 25.60 25.80 I • • i1 “ ‘h rrrMY ■ Hr + > I ■ >| 111111. ■ 11 > ■.. ।. 11 ■ 111 mmPrl I j > ।. 11 ।, T’TI m/z 189.10 14.58% miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 1118

5000 113 TIt*‘*I* 25.20 25.40 25.60 25.80 m/z 79.90 13.01% 80 94 160

miz-> 66 ■ • i ■ • ■ ■ i • • ‘ ■ i ■ ■' ■ i “ ‘ — 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 . ... w.. Abundance #19957: Anthracene-d10- 11)8 .... ..... ........... .

25.20 25.40 25.60 25.80 5000 m/z 187.25 11.78%

. 80 94 160 66 । miz-> ---H 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19908: Naphthalene, 2,6-dimethoxy- 1118 1 25.20 25.40 25.60 25.80 173 m/z -94.00 11.47% 145 5000 102 114 130 76 94 — TITpt ______________ *** m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.20 25.40 25.60 25.80

12571.D GCMS0531.M Tue Jun 04 11:52:48 2002 Page 2

NYC-WTC_000014698

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NYC-WTC_000014698Source: NYC Law Department, mirrored locally

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