GCMS analysis results for sample AE07501, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \HPCHEM\ 1 \DATA\APR18027501.D Vial: 9 Acq On : 20 Apr 2002 1:24 am Operator: Sample : gc/ms scan 4/1 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 25.73 0.20 ug/1 34678 Phenanthrene-dl0 25.59 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-d1o K 4 188 C14D10 001517-22-2 2 Anthracene-dl0 - 188 C14D10 / 001719-06-8 91 3 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 40 4 Naphthalene, 1,7-dimethoxy - 188 C12H1202 005309-18-2 40 Abundance 7 Scan 2253 (25.729 min): 7501 .D (-) m/z 188.10 100.00% 188

5000

........... ........... .......................... ■ ' । ' 1 r ' ।1 1 1 ' । 1 ■ ■ 1 । 1 1 1 1 i 80 94 44 66 158 25.40 25.60 25.80 26.00 ' " i ■''' i11111''111'1 T ■ i ‘1'' i1'1111111 r '1' i ■' I'111' " i1''' i' 4 — m/z 184.10 15.76% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

5000 25.40 25.60 25.80 26.00 m/z 80.05 15.29% 80 94 160 66 000010000101111/11 —..... m/z-> A 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188 - 25.40 25.60 25.80 26.00 5000 m/z 189.05 13.15%

160 —1WWTTTTTTITPTPTTTTTTTTTTT 66 7 9i 'i11111 rl 111 m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69165: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime .......... , 188 25.40 25.60 25.80 26.00 m/ Z 94.00 12.44%

5000

143 64 89 116 130 158 170 m/z—> ■' । ■ ■ ■ ■ । ‘ 40 50 60 70 ■ ■ । 80 90 100 110 120 130 140 150 160 170 180 190 ■ 11 <-i । > 1111111 ■ ITT | J1 i ' 25.40 25.60 25.80 26.00

7501.D GCMS0419.M Mon Apr 22 10:43:50 2002 Page 2

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