GCMS analysis results for sample AE07501, April 2002

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DEP laboratory report showing GCMS analysis results for sample AE07501 conducted on April 23, 2002.

NYC-WTC_000047034–000047043

Folder label: “GCMS X 4/1/02 A 4/19/02”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\l\DATA\APR1802\7501.D Vial: 9 Acq On : 20 Apr 2002 1:24 am Operator: Sample : gc/ms scan 4/1 fb Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 1,3-Dioxolane, 2-pentadecyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

8.11 0.29 ug/1 35030 1,4-Dichlorobenzene-d4 12.22 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane, 2-pentadecyl- 284 C18H3602 004360-57-0 9 2 2,2 1 -Trimethylenebis- 1,3-dioxolane 188 C9H1604 006543-04-0 9 3 2-Methyl-/-hexen-3-ol 114 C7H140 032815-70-6 9 4 N-Ethylformamide__________________73 C3H7NO 000627-45-2 5 Abundance ’ Scan 334 (8.112 min): 7501 .D (-) m/ z 73.00 100.00% 73

5000 43 1*** 7.80 8.00 8.20 8.40 571 87 103 ' ' r 1 1 ' P ' 1 ' 1 1 ' ' 1 I ' ' ' ' I 1 1 1 ' I ' 1 1 1 1 17" i | . . . ' | . i | i I r^i . ( , , , | . i i i I > -I i i I i i m/z 42.95 26.60% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #40191:1,3-Dioxolane, 2-pentadecyl- 73

5000 7.80 8.00 8.20 8.40 m/ z 45.05 9.02% 43 57 86 99 256 283 - ■ i ■ ■ ■ ■ । ■ I ' ' ' ' | 1 1 11 | ■ 1 11 | 1 1 1 1 I ‘T‘ । | । । i । | । i । i । 1 . । । . i । । । ri i i । 'i i m/z->____ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #19777: 2,2'-Trimethylenebis-1,3-dioxolane 73 ... Ill.... —' 1 1 I ' ' 1 1 I 1 ' 1 ' I ' ' ' ' I ' ' ‘ 1 I 7.80 8.00 8.20 8.40 5000 m/ z 41.05 7.76% 45 29 99 145 11. HI, I ‘ I’’’’ I 1 ' 1 1 i ' ' ' ■ । > > ■ ■ । • ■ ■ ■ । • ■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । । 1 • > • । ■ • ■ ■ । > 1 । > > > ■ । ■ ■ m/z—>_____ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #3017: 2-Methyl-5-hexen-3-ol 73 7.80 8.00 8.20 8.40 55 m/z 71.00 7.38% 5000

m/z—> ...4, 20 27

40 I , , 1 ....... ... 1 | । 60 .... I ! I | !. ............... ' 1 ' ' ' ' I ' ' ' ' I ' ' ' ' 1 ' ' ' ' I 80 I I I | , I I ! p, I I 100 120 140 160 180 200 220 240 260 280 | II I I | I I I I | U 1 i

7.80 | ' ■ i ।

8.00 | r i i I

8.20 | I I I I

8.40 | I I I I J

7501.D GCMS0419.M Mon Apr 22 10:43:50 2002 Page 1

NYC-WTC_000047041

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NYC-WTC_000047041Source: NYC Law Department, mirrored locally

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NYC-WTC_000047101

DEP laboratory report showing GCMS unknowns analysis results for sample AE07486 conducted on April 23, 2002.

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