GCMS analysis results for sample AD31591, Feb 28 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\31591.D Vial: 38 Acq On : 23 Feb 2002 3:36 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 2 09 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 1,3-Dioxolane, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 3.15 ug/1 247537 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3 -Dioxolane , 2-methyl- 88 C4H802 000497-26-7 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1, 3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 Pentane,/3-methoxy- 102 C6H140 036839-67-5 9 Abundance Scan 344 (8.204 min): 31591.D (-) m/ z 73.00 100.00% 73

5000 43

7.80 ; 00 8.20 8.40 8.60 381 1 49 5,5 ....... , TIttu TTdTTIT........ . 1 87 103 ■ i ■ ■ ■ ■ i ' • • • i ■ m/ z 43.0.5 29.84% miz-> 10 20 30 40 50 60 7( 80 90 100 11 120 Abundance #62902: 1,3-Dioxolarie, 2-methyl- 73

5000 43 I 7.80 8.00 8.20 8.40 8.60 I 53 m/z 44.95 10.93% 87 27 I — -PI — -+ — I ■ ■ ■ • i 1 ■ ■ ■ i 1 ' ' ' i ' ' i ' ■ ' ' i ■ ■ ■ ■ i ’ ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292; N-Ethylformamide 30 73 —1 , . 1111 -1-. r TT r 7.80 8.00 8.20__ 8.40 8.60 5000 m/ z 41.05 10.18% 44 58

15 ! | । ; I................ ' ' ' I ' ' ' .................। । । । ............................... ... , m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet 73 7.80 8.00 8.20 8.40 8.60 m/ Z 71.00 6.14% 5000

45 36 55 11 . > . TIPPI■ I । • | ' ' . I . . . . I . . 67, ■ ■ i ■ 109 115 I I mI I TIPAT I—II I I I miz-> 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 .20 8.40 8.60

31591.D GCMS0208.M Wed Feb 27 12:06:03 2002 Page 1

NYC-WTC_000038212