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GCMS analysis results for sample AD31591, Feb 28 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31591 conducted on February 28, 2002.

NYC-WTC_000038205–000038219

Folder label: “GCMS X 2/21/02 A 2/22/02

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Scanned page image, NYC-WTC_000038213
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\31591.D Vial: 38 Acq On : 23 Feb 2002 3:36 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Pentanal Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

8.26 0.47 ug/1 37019 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 .Tentative ID MW MolForm CAS# Qual

1 Pentanal 86 C5H10O 000110-62-3 4 2 Acetaldehyde 44 C2H40 000075-07-0 3 3 Carbon /dioxide 44 CO2 000124-38-9 3 4 Ethyne, fluoro­ 44 C2HF 002713-09-9 3 Abundance Scan 350 (8.259 min): 31591.D (-) m/z 39.95 100.00% । 40 i 44

5000

1IT TTT TT 36 8.00 8.20 8.40 8.60 51 86 I TH+ I"" . ..... 1' • • i ’ "111 • ‘11 •1'11'11 • i1 i" " i IBOUI—TTu m/z 43.95 71.67% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #692: Pentanal 44 29

5000- 41 58 8.00 8.20 8.40 8.60 15 m/z 36.00 3.20% 26

m/z-> 5 - 10 i ■ ■'11 38 L 15 20 25 30 35 40 45 50 55 60 65 70 75 80 ■ r " ' i 'i""r 86 i ■1" i TT 85 90 95 Abundance #62264: Acetaldehyde 29 44

8.00 8.20 8.40 8.60 5000- m/ Z 43 . 00 2.17%

26 Ti i• i '11' r " 11'11' i1 111 •' I 11 ‘ 41 : ■ i •1 ■ • i ■ M ■ i ■ ■ " r ■ " i ■ ■ " r i1' •' i I’ m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 'Abundance #34: Carbon dioxide 44 8.00 8.20 8.40 8.60 m/z 38.05 1.74% 5000-

16 22 I ‘ ■ "i ■ ‘' I ’' ” I' ‘" I " " I ’ ' I " •' I TTT i1 ‘" i | I I | I I I I | lik. । i . . > । ■ i > i | TT m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 8.00 8.20 8.40 8.60

31591.D GCMS0208.M Wed Feb 27 12:06:07 2002 Page 2 NYC-WTC_000038213

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NYC-WTC_000038213Source: NYC Law Department, mirrored locally

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