GCMS analysis results for sample AE03335, Mar 15 2002

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Data File : C:\HPCHEM\1\DATA\FEB2102\3835.D Vial : 75 Acq On : 24 Feb 2002 7:50 pm Operator: Sample : gc/ms scan 2/22 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane, 2-(3-bromo-5,5, Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 4.01 ug/1 263027 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane/ 2-(3-bromo-5,5,5-tri•352 C10H16BrC13O2 000000-00-0 23 2 N-Ethylformamide 73. C3H7NO 000627-45-2 9 3 Silane, tetramethyl - 88 C4H12Si 000075-76-3 9 4 Pentane, B-methoxy- 102 C6H140 036839-67-5 9 'Abundance Scan 344 (8.197 min): 3835.D (-) m/z 73.00 100.00% 713 ■

5000 43 7.80 8.00 8.20 8.40 8.60 67, J 1.... 87 ..... 103........ m/z-> i ■ ' ■ ' i ' ' ' ' i 1 10 20 30 — 40 50 560 70 80 90 ■ • i • 100 110 120 m/z 42.9,5 31.12% Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet 73

5000 1 1 1 r ' i • ■ ■ ' i ■ 7.80 8.00 8.20 8.40 8.60 45 m/z 41.05 11.43% 55 67 , -mmm36 1 I ' 1 ' ■ । • l • ■ > ■ i > • • • i ■ ........................ 109 115 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 . i 73 7.80 .. q —Pn.. 8.00 8.20 8.40 8.60 5000 m/z 44.9.5 11.37% 44 58

15 ; ; - 1 , r-j-r-r-r m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62932: Silane, tetramethyl- 7)3 7.80 8.00 8.20 8.40 8.60 m/ Z 71.00 6.70% 5000

45 | .53 59 15 ■ ■ । ■ ■' ■ > i ■ ■ • ■ । ■ । । । I Hi । । I ।......... 88........................... m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40 8.60

3835.D GCMS0208.M Wed Mar 13 11:34:50 2002 Page 1

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