Laboratory report documenting GCMS analysis of sample AE05847 conducted on April 17, 2002, including surrogate recovery data.
NYC-WTC_000059619–000059628Folder label: “GCMS X 3/12/02 A 4/4/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\APR0402\5848.D Vial: 22 Acq On 4 Apr 2002 6:47 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane, 2-(3-bromo-5,5, Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
8.12 7.56 ug/1 338609 1,4-Dichlorobenzene-d4 12.24
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,3-Dio^lane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 17 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 N-Ethy/formamide 73 C3H7NO 000627-45-2 9 4 1,3-Di/oxolane, 2-pentadecyl- 284 C18H36O2 004360-57-0 9 Abundance Scan 335 (8.119 min): 5848.D (-) m/^ 73700 100.00%| 713 ft 5000 43 ■n" 87 7.80 8.00 8.20 8.40 ■?■■■. . .57, I 103 I ' ' ' ' I ' ' ' ' I ' ' I I ' ' ' I '' I ' ' ' ' I ' I ' ' i'' ' ''■ I ' m/z 43.05 30.01% Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423:1,3-Dioxolane, 2-(3-bromo-5.5,5-trichloro-2,2-dimet 713
-rT-ry-r-r-i-t-I-rT^T-rj-T-r-r-i=f=i=^^ 7.80 8.00 8.20 8.40 45 m/z 41.05 10.19% t....... ?........... ^,.,1,1 55 67, '“I ' ' • • I.' ' ' ' I ' ,109J15 Ti/z-> 10 20 30 40 50 60 70 80^ 90 100 110 120 Abundance #763; 1-Butanamine, 3-methyl- 33
7.80 8.00 8.20 8.40 5000 m/z 45.05 9.81%
m/z-> Abundance 10 15 20 30 33. 41 'V++ 40 50 55 60 70.... y,., • 70 #292: N-Ethylformamide
73 80 90 100. 110 120 _L m/z 7.80 8.00 71.00 8.20 8.40 7?^^
5000 44 58
m/z-> 10 20 ■I 30 ....40'I'l....50 60 70 80 90 100 110 120 7 80 8 00 8 20 8 40
5848.D GCMS0408.M Tue Apr 16 08:17:23 2002 Page 1
NYC-WTC_000059626
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NYC-WTC_000059629
Laboratory report documenting GCMS analysis of sample AE05848 conducted on April 17, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059650
Laboratory report documenting GCMS analysis of sample AE05851 conducted on April 17, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059555
Laboratory report documenting GCMS analysis of sample AE05745 conducted on April 11, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059608
Reference data report listing component names and response values for calibration verification conducted on April 16, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059526
Laboratory report documenting GCMS analysis of sample AE05703 conducted on April 11, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059286
Laboratory record of gas chromatography mass spectrometry analysis for unknown compounds and surrogates on April 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058372
Analytical run record from April 2, 2002, documenting unknown compounds and surrogate recovery for sample AE04590.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059565
Laboratory report documenting GCMS analysis of sample AE05746 conducted on April 11, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059639
Laboratory report documenting GCMS analysis of sample AE05849 conducted on April 17, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011757
Laboratory report documenting GCMS analysis of sample AE04127 conducted on April 1, 2002, by analyst DLV.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039535
Laboratory report documenting GCMS analysis of sample AE06451 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047119
DEP laboratory report showing GCMS analysis results for sample AE07488 conducted on April 23, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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Technical record detailing laboratory method parameters including drip rates and reagent volumes for sample processing.
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Laboratory report showing GCMS blank analysis results for sample AE05847 conducted on April 16, 2002, with compound detection limits.
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NYC-WTC_000059603
Calibration report listing detector response values and minimum detection levels for various organic compounds analyzed on April 16, 2002.
Filed in the same folder