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GCMS analysis results, sample AE05233, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE05233 for unknown compounds on April 9, 2002.

NYC-WTC_000059145–000059155

Folder label: “GCMS X 3/9/02 A 3/30/02

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Scanned page image, NYC-WTC_000059152
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5233.D Vial: 44 Acq On : 31 Mar 2002 11:38 am Operator: Sample : gc/ms scan 3/9 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★if********

Peak Number 1 1,3-Dioxolane, 2-(3-bromo-5,5, Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.13 0.78 ug/1 90712 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 23 2 1-Butanamime, 3-methyl- 87 C5H13N 000107-85-7 9 3 Pentane, 3/-methoxy- 102 C6H14O 036839-67-5 9 4 2 - Propanoi/ie, oxime 73 C3H7NO 000127-06-0 7 Abundance Scan lie (8.132 min): 5233.D (-) m/ z 73 700 7|3

5000 1 43 T 55 87 103 7.80 8.00 8.20 i8.40 ......... ................. , ,,, , I ‘ I ' ' ' ‘I' 4-^ m/ z 43.05 30.15% __ 10 20 30 40 50 60 70 80 90 100 . 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5.5,5-trichioro-2,2-dimet 7)3

5000 7.80 8.00 8.20 8.40 45 m/z 45.0,5 10.68% 3^ I I I 55 67. ,________________ 109 115 ' I ‘ ' I ' ' ' ' I ' ‘ ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' m/z-> 10____ 20 30 40 50 60 70 80 90 100 110 120 Abundance #763; 1-Sutanamine. 3-methyl- 30 -T-r-rA-r-r-rT-rl^^

7.80 8.00 8.20 8.40 5000 m/z 41.05 10.45%

IS 41 55 70 87 r-pr-r-r- ' I'''' I ' '' ' I'''' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' 1 ' ' ' ' I ' ni/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #1793; Pentane, 3-methoxy- /V ' I ' ' ' ' I 7)3 7.80 8.00 8.20 840_____ m/z 71.00 7.20% 5000 45

Y 33 39, 55 , ........ i ' I ' ''' ' I ' ' ' ' I I 10 20 30 40 50 60 70 80 90 100 ' 110 120 7.80 8.00 8.20 8.40

5233.D GCMS0308.M Wed Apr 03 13:57:16 2002 Page 1

NYC-WTC_000059152

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NYC-WTC_000059152Source: NYC Law Department, mirrored locally

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