GCMS analysis results for sample AE02598, Mar 2002

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Data File C:\HPCHEM\l\DATA\MAR0102\2598.D Vial: 8 Acq On l Mar 2002 3:14 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane, 2-(phenylmethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.20 0.38 ug/1 32263 1,4-Dichlorobenzene-d4 12.31

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane, 2-(phenylmethyl)- 164 C10H12O2 000101-49-5 9 2 3 -Pentano 1, 3-methyl- 102 C6H140 000077-74-7 9 3 1,3-Dioxolane 74 C3H602 000646-06-0 7 4 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 7 Abundance ' Scan 344 (8.200 min): 2598.D (-) : m/z 73.00 100.00% 73

5000 43 ) 7.80 8.00__ 8.20 8.40 8.60 41 55. 11141’ t' 1111111 ’14 । " r PTi 87 103 T1*mpmmpp m/z 43.05 7 26.74% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #13422: 1,3-Dioxolane, 2-(phenylmethyl)- 73 ............ /..

5000 7.80 8.00 8.20 8.40 8.60 91 m/ z 41.0,5 11.76% 45 65 I ' 103 120 • "64 TIOItuu—DDTIT i' r 1 ' i' miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance 73 - I ■ i ■ ■ 7.80 8.00 8.20 8.40 8.60 5000 i m/z 44.95 11.07% — 45 55 27 87 ‘ I‘‘‘‘1‘I‘II‘+‘II‘‘‘II-‘AII‘A‘II‘‘ISI‘‘LISSI/II/IIICII|I|II||* m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #62557: 1,3-Dioxolane............................... 73 7.80 8.00 8.20 8.40 8.60 29 m/ Z 71.00 7.51% 44 5000

15

m/z-> - 10 20 + 30 TTT " । " ■11■" 11 ‘1'' i1 ■1 ■ i ■" ■ i1111111111111' i " " i 40 50 60 70 80 90 100 110 120 130 140 150 160 170 i 7.80 8.00 11' ■ ■ । ■ ■ ■ ■ । • 1 i 1 ' 8.20 8.40 8.60

2598.D GCMS0208.M Mon Mar 04 11:42:30 2002 Page 1

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