GCMS calibration table for TCLP method, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C : \HPCHEM\ 1 \DATA\MARO 102\3265.D Vial: 40 Acq On 3 Mar 2002 2:39 am Operator: Sample gc/ms scan 2/4 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.19 1.57 ug/1 308338 1,4-Dichlorobenzene-d4 12.32

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 N-Ethylformamide 73 C3H7NO 000627-45-2 9 Abundance t Scan 342 (8.186 mln): 3265.D (-) m/ z 73.00 100.00% 73

5000 43 *IBBaLP/I1LL.u 1 n 11 11 i 11 7.80 8.00 8.20 8.40 8.60

m/z~> ---PPPPP344 10 20 30 40 — 50 50 55 • i • • 60 70 । I i • • ■ * r• 80 , 87 90 100 103 110 m/z 42.95 29.40% Abundance #62902:1,3-Dioxolane, 2-methyl- 73

5000 43 7.80 8.00 8.20 8.40 8.60 58 m/z 44.95 10.80% 27 87 1 ■ i ■ ■ • ■ i 1 ■ r) I1" ■ ' I 1 • • I ' ' i ■ ■ ■ ■ i ■ 1 ■ ■ i ' 1 ' ■ i ■ • ■ ■ i ■ ' ■ ■ i ' miz—> 10 20 30 40 50 60 70 80 90 100 110 Abundance 32 Siane strameth 73

7.80 8.00 8.20 8.40 8.60 5000 m/z 41.05 10.25%

45 15............... 1 121/88." i । j i i 53 59 88 j i i‘« ■ i ■ ■' i • ' • ■ i ■ • ■ ■ i ■ ■ • 1 i ' ' 1 1 1 1 1 ‘ ' I ‘ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763:1-Butanamine, 3-methyl- 33 7.80 8.00 8.20 8.40 8.60 m/Z 71.00 6.77% 5000

15 41 55 70 87 X Tr IIIa.n .[•<■. 11 I . |"> ■ i r | ■ । । । | i m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

3265.D GCMS0208.M Mon Mar 25 12:16:34 2002 Page 1

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