GCMS sample analysis results, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30256.D Vial: 17 Acq On : 29 Dec 2001 2:47 pm Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane, 2-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

7.62 2.82 ug/1 767028 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 Butane, 2/methoxy-2-methyl- 102 C6H140 000994-05-8 9 Abundance Scan 280 (7,617 min): 30256.D (-) m/z 73.00 1 00.00% 73

5000 43 1*’’’I**’*I*’I*’**I** 7.20 7.40 7.60 7.80 8.00

miz-> 10 . ................. 20 30 39,1,1,1, 40 50,-589,1118741, 50 60 70 , ’I 1 i 1 80 87 । 90 103 ' i'1' । ' i > 100 110 rn/z 43.00 33.04% Abundance #62902:1,3-Dioxolane, 2-methyl- 73

5000 43 7.20 7.40 7.60 7.80 8.00 58 m/ z 45.0.5 11.99% 27 87 1, I1" ' ■ I । ' 1 I ' ' i ■ ■ ■ ■ i • 1 ■ ‘ i ■ ■ ' ■ i ■ ■ 1 ■ i ■ ■ ■ ■ i • miz-s 10 20 30 40 50 60 70 80 90 100 110 (Abundance #763: 1-Butanamine, 3-methyl- 30 —rr 1tn 111 ■ IUmT n 1" 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.05 11.11%

15 4155 70 87 III’IIIIFII ■ ■ l 1 ■ ■ ■ i ■ ■ ■ ■ i ' 1 • 1 i ' • i ■ m/z->_____ 10 20 30 40 50 60 70 80 90 100 110 _ . — .... Abundance............ #845: Silane, tetramethyl- DBGGTTE—SOm—B—nnmnm- 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.87% 5000

45 15 31 , ,1 55 88 I ■ • i • ‘ ■ 1 i • ■ ■ ■ i ' • TT—RRTT TTIt ■ 1 i ■ ■ ' 1 i ' 1 ■ ■ I ■ • ‘ ■ i • =_11dasana (r t , miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30256.D GCMS1126.M Wed Jan 02 10:24:12 2002 Page 1

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