GCMS analysis results for sample AD31347, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1502\31347.D Vial: 10 Acq On : 15 Jan 2002 7:45 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.44 4.09 ug/1 926633 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 Abundance Scan 261 (7.442 min): 31347.D (-) m/ z 73.0.0 100.00% 73

5000 43

103 ' ■ i ■ 7.00 7.20 7.40 7.60 7.80 . 38.1, .1, 50 55,60 67, 1 ,I 1 ■ i ■ ‘ 87 ' ■ i ■ ' ■ ■ i ■ ■ ■ • i ■ • 1 ’ I ’ 1 1 ’ i’ * ‘111 iI r ' ■ • l • ''' 1 1 ■ ■ ■ i m/z 43.00 32.77% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902:1,3-Dioxolane, 2-methyl- 73

5000 43 |+*’’1’4+’14*’’t+4*’I’’ 7.00 7.20 7.40 7.60 7.80 58 87 m/z 41.05 12.09% . 27 a m/z->_____ 10_.... 20____ 30___ 40 ■ ■ i ‘ 1 1 ‘ i ' ■ ‘ ■ i ■ 1 ■ ■ i ■ ■ ■ ■ i ' 1 ■ ■ i ■ ■ ■ ■ i ' 50 60 70 80 90 100 110 Abundance #202; N-Etylformenc 30 73 "I 174 i ITT । i |*> । । i 11 " rp r I t 7.00 7.20 7.40 7.60 7.80 5000 m/ z 45.05 11.74% 44 58

15 L* m/z-> 10 20___ 30__ 40 50 60 70 80 90___100__ 110 Abundance #763: 1-Butanamine, 3-methyl- — T -u ■ rr f FTrru ' 30 7.00 7.20 7.40 7.60 7.80 m/ z 71.00 6.61% 5000

15 41 , 55 ' i ■ ■ ■ ■ 70 87 i 1 ' ■ ■ i * ■ ' ■ i ■ ‘ ' i ' ‘ I ■ • ■ ■ ■ i 1 1 ■ ■ i ■ I 1 1 ■ ■ i ' 1 .pri , p . । r, m/z->_____ 10 20 30 40 50 60 70 80 90 100 110 7.00 7.20 7.40 7.60 7.80

31347.D GCMS1126.M Mon Feb 04 15:02:17 2002 Page 1

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