GCMS analysis results for sample AD31347, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1502\31347.D Vial: 10 Acq On : 15 Jan 2002 7:45 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.14 0.42 ug/1 121605 Naphthalene-d8 15.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasi loxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 Benzeneetham line, N- [ (pentafluorop 563 C24H34F5NO3S13 055429-13-5 43 3 3,4 - Dihydroy ybenzyl alcohol,tris(tr 356 C16H32O3S13 068595-79-9 38 _4 Benzoic acid , 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 32 Abundance Scan 991 (14.144 mln): 31347.D (-) m/ z 73.00... 100.00% 73

5000 267 355 45 13.80 14.00 14.20 14.40 119 154 193 223 , 323• ’ i* 1 ' ' i • ■ ‘ ■ i 1 ■ ■ ' i • ■ ‘ ‘ l 1 1 1 45 m/z 267.0.0 38.02% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 13.80 14.00 14.20 14.40 m/z 355.05 25.57% 207 , a 323, • • i • ■ ■ • i • ■ ■ ‘ i • ■ ■ ■ i • ■ ■ ■ i ' ■ ‘ ■ i ' ■' ‘ ■ i ■ ■ 1 ■ i ‘ 1 ■ ■ i • ■ ‘ ■ i ■ ■ ■ ■ i ‘ ■

m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance —i or ■ 6* : 0 • J . Attpomtofuenggnong isctecj 73 355 13.80 14.00 14.20 14.40 5000 m/z 356.05 9.74%

45 208 251 281 386 458 548 mfz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 13.80 14.00 14.20 14.40 m/z 267.90 9.27% 267 5000 179 356 45 147 209 237, 312■ ' ‘ i ‘ ‘ i ‘ ‘ ■ i ' ' 1 ■ i ■ ■ ■ ■ i ' ' ■ ‘i ‘ ■ 11 r' 1 1 1 । 1 1 ' • i • i ■ । ■ ■ i ' ' i • ‘ • i ■ • ■ ■ i ' • ■ ■ i m/z-> 50 100 150 200 250 300 350 400 450 500 550 13.80 14.00 14.20 14.40

31347.D GCMS1126.M Mon Feb 04 15:02:22 2002 Page 2

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