GCMS analysis report, sample AE04419, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAR2102\4419.D Vial: 10 Acq On : 21 Mar 2002 8:09 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.14 2.05 ug/1 313687 1,4-Dichlorobenzene-d4 12.27

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 1,3-DioxoLane, 2-methyl- 88 C4H802 000497-26-7 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 Thiocyanic acid, methyl ester 73 C2H3NS 000556-64-9 4 Abundance Scan 337 (8.137 min): 4419.D (-) m/ z 73.00 1 00.00% 73

5000 43 ..... L..... 7.80 8.00 8.20 8.40 3? |, | 50 55 67i , [....... 87 ........ 193, , 11 m/z 29.20% miz-> 10 20 30 40 50 60 70 80 90 100 ’ 110 Abundance #62902:1,3-Dioxolane, 2-methyl- 73

5000 43 TT ■ ■ ■ i 7.80 8.00 8.20 8.40 58 87 m/ z 45.05 10.76% 27 ■11 i ■ ■ ■ ■ i 1 1 ' ■ i ■ 1 ■ ■ i ■ • • • i ■ i ■ ■ • ■ i ' 1 ■ ' i 1 ■ ■ ' i ' ■ ■ ‘ i ■ ■ ■ ■ i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance ‘-Ethylformamige 30 73 *’1***’I’ 7.80 8.00 8.20 8.40 5000 m/z 41.0 10.08% 44 58

15 1/001001*0 miz-> 10 20 30 40 50 60 70 80 90__ 100 110 Abundance #62932: Silane, tetramethyl- ' 1 1 10M « । . i , । i 11 । T'i i । । 73 7.80 8.00 8.20 8.40 m/z 71.00 6.31% 5000

45 15 , J 53 59 88 .................. ■ ■ i ■ ' i 1 ■' 1 •"I 1 1 --1-1 ■ ■ i ■ ■ ■ ' i ' ■ ■ ■ i ■ ‘ ■ i ' ‘ ‘ I ' ' ' 1 I ' ' ■ ' I ' ' r' I ‘ ‘ ■ I m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

4419.D GCMS0308.M Fri Mar 22 09:41:48 2002 Page 1

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