GCMS analysis report, sample AE04419, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2102\4419.D Vial: 10 Acq On : 21 Mar 2002 8:09 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Oxirane, [(1-methylethoxy)meth Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

8.24 0.38 ug/1 57831 1,4-Dichlorobenzene-d4 12.27

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, [ (1-methylethoxy) methyl] - 116 C6H1202 004016-14-2 9 2 Acetone 58 C3H6O 000067-64-1 7 3 Propanal 58 C3H60 000123-38-6 7 4 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 5 Abundance Scan 348 (8.238 min): 4419.D (-) m/z 42.. 95 100.00% 413 59 5000 101 —TTT 38 7.80 8.00 8.20 8.40 8.60 --------- 10 20 30 40 50 60 70 i-nir II.. 4... 80 90 -myv 100 110 m/z 59.05 67.27% Abundance #64267: Oxirane, [(1-methylethoxy)methyl]- 43 59 /VY /______ 5000 27 i ‘ ' i ‘ ■ i ‘ ‘ ‘ ' i ' ' ‘ ‘ i ‘ ' 7.80 8.00 8.20 8.40 8.60 101 m/z 100.9 24.87% 73 . ! ; 86 । > r> > । > i > i > । । 1 1 ' I 1 1 ■ ■ i • • ‘ ■ i ■ ■ 1 ■ i • ■ ■ • i ■ ■ ■ ■ i ■ ‘ • i ■ ■ ■ 1 i ■ m/z-> 10 20 30 40 50 60 70 80 _ 90 100 110 Abundance #94: Acetone 43 I ' • ‘ ‘ I ‘ ‘ ' I ‘ ‘ ‘ 1 1 ‘ ‘ * 1 1 1 ‘ 7.80 8.00 8.20 8.40 8.60 5000 m/z 58.05 23.59% 15 58 27 ■ । ■ ■ ■ • i ' ■ ■ ■ i ■ ‘ ■ • i ■ ■ ■ ■ i ' ■ I ■ ■ ■ ■ i 1 ■ ■ ■ i 1 1 • • i ■ • • ■ i ■ ‘ ‘ ■ i ‘ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62333: Propanal *11 * 4 * i • * 1 * i * ■ * * i * > 29 7.80 8.00 8.20 8.40 8.60 m/z 40.95 6.61% 5000 58

miz-> • ■ i 1 ■ 1 1 i ■ 1 10 20 -pl 30 40 50 60 70 80 90 100 110 7.80 । 71 . । > । A i । । IT । Pi । । । i > 8.00 8.20 8.40 8.60

4419.D GCMS0308.M Fri Mar 22 09:41:53 2002 Page 2

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