GCMS analysis results for sample AE08017, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR1102\8017.D Vial: 23 Acq On : 12 Apr 2002 12:01 pm Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Oxirane, [(1-methylethoxy)meth Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.22 0.40 ug/1 51415 1,4-Dichlorobenzene-d4 12.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxiranes, [ (1-methylethoxy) methyl] - 116 C6H1202 004016-14-2 40 2 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 33 3 2-Propanone, 1-cyclopropyl- 98 C6H10O 004160-75-2 7 4 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 7 Abundance Scan 346 (8.219 min): 8017. D (-) m/z 42.95 100.00% 43

59 5000-

101 * tIrm Mt । *I । i । । TrTTi er 7.80 8.00 8.20 8.40 8.60 T" 111 I"■■ l < >111 +495 83 i ‘ ' i " " r 1" r " 11" 11 r ‘ " r " ‘ i " 1' i1" ■ i ■■ "i1 i m/z 59.05 54.93% n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #64267: Oxirane, [(l-methylethoxy)methyl]- 43 59

5000 । ■ r ■ । ■ ■ ■ ■ । । । ■ ■ ■ ■ । ■ 27 7.80 8.00 8.20 8.40 8.60 101 m/z 101.05 19.67% 73 I■>■• ।■ ■ ■ ■। ■I■। 86 ‘ । ।1 " 11" 111 TTf 1" r 1" i1 r " ' i " " r 1111 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43 7.80 8.00 8.20 8.40 8.60 5000 m/z 58.05 18.31% 59

27 101 49 . 83 ।। ■ I ■11■ ■ ■ ( mrplijl.. . +PTT+ TTT r m/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105

43 #1306: 2-Propanone, 1-cyclopropyl- 1 ' • n M rI ' 1 ' 1 1 1 ' ' ' I ' ' 7.80 8.00 8.20 840 8.60 m/z 41.05 8.04%

5000

m/z—> 29 55

r ' " 1 | ' । - । | " ■ ■ | । > । । | । । 11'1111" । ■ 1 । । | 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 69 83 98 | । I | । I <T| " । 1 | " 1 I | । । " | 1 > " | 1 । । 1 | " । । | 1 । 1 l| । 7.80 8.00 8.20 L 8.40 8.60

8017.D GCMS0412.M Tue Apr 16 12:08:23 2002 Page 1

NYC-WTC_000047722