GCMS analysis results sample AD29299, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1201\29299.D Vial: 29 Acq On 13 Dec 2001 5:18 am Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 1,3-Dioxolane, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.59 3.90 ug/1 1195260 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane,2-methyl- 88 C4H802 000497-26-7 9 2 N-Ethylformajm.de 73 C3H7NO 000627-45-2 9 3 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 Abundance 4 Scan 278 (7.593 min): 29299.D (-) m/ z 73.0,0 100.00% 73

5000 43

37. |, | 55 61 67, । | 78 87 .........103.............. 7.20 7.40 ' 780 7.80 8.007 1 i ' ■ ■ ■ i ' > i > • • ■ । । । ■ . । . * • ■ ■ ■ TIT m/z 43.0.0 26.30% m/z-> 10 20 30 40 50 60 70 80 90 100 11G 120 Abundance #62902: 1,3-Dioxolane, 2-methyl- 73

5000- 43 7.20 7.40 7.60 7.80 8.00 58 m/ z 44.9.5 10.32%

m/z-> 27 .............. — L i........... । 10 20 30 40 +.. 50 ■ । > । * > । * 60 70 80 4 87

90 100 110 120 Abundance #292: N-Ethylformamide 30 I 73 i 1 ■ ■ r ■ l ■ TIT 1 7.20 7.40 7.60 7.80 8.00 5000- m/z 41.00 9.76% 44 58

15 ........ '............ I . ' ■ i 1 ' ■ ■ I ■ ■ ■ 1 i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet TTT | 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.0.0 6.56% 5000-

45 ................ 3611 ■ i > » ■ i • • ■ ■ । । । 55 67, • ■ ■ i • ■ ■ ■ i • • ■ • i ■ + ............. 109115 T IT II—-rr+j-—IT Imm miz-> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 1.00

29299.D GCMS1126.M Fri Dec 21 12:22:01 2001 Page 1

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