GCMS analysis results for sample AD31587, Feb 28 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\FEB2102\31587.D Vial: 34 Acq On 22 Feb 2002 11:40 pm Operator: Sample gc/ms scan 2/21 Inst : GC/MS 209 Misc. Multiplr: 1.00 • MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.88 0.22 ug/1 22848 Phenanthrene-dl0 25.73

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-d10 188 C14D10 001517-22-2 78 2 Anthracene-d10- 188 C14D10 001719-06-8 72 3 2-Quinolinecarboxaldehyde. 8-hydrox 188 C10H8N2O2 005603-22-5 45 4 Antipyrine 188 C11H12N2O 000060-80-0 36 'Abundance 7 in 2270 (25,880 min): 31587.D (-) m/z 188.10 100.00% 188

5000

. 94 158 , 25.60 25.80 26.00 26.20 66 78 | — • ■ । ■ I ■ । ■ ■ ■ 11 ■ ■.. i11 ■. । ■ m/z 189.10 18.10% m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 'Abundance #19958: Phenanthrene-d10 188

___________ 5000 • ' i ■ ' ■ ■ i ' 1 ■ ' i 25.60 25.80 26.00 26.20 m/ Z 94.00 15.37% __ 80 94 160 ——— i 66 I ,I.................................... — m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- i 188 ___ / V ■ ■ I ■ J ■ ■ I < I 25.60 25.80 26.00 26.20 5000 - m/ z 158.15 14.37%

80 94 160 66 ■ 1 1 i • > * * i > I, .m/z-> 60 70 80__ 90 100 110 120 130 140 150 160 170 180 190 Abundance #69165: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime ‘i V 188 25.60 25.80 26.00 26.20 m/z 184.10 10.87%

5000- 143

miz-> — 64 60 70 ...... 7 ... .... 116130 — 158 170 IHP — 80 90 100 110 120 130 140 150 160 170 180 190 tt । / , r i । r-r 25.60 25.80 26.00 26.20

31587.D GCMS0208.M Wed Feb 27 12:02:38 2002 Page 2 NYC-WTC_000038175