GCMS analysis results for sample AD31587, Feb 28 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\31587.D Vial: 34 Acq On : 22 Feb 2002 11:40 pm Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 3.64 ug/1 292280 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 17 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Pentane, 3 -methoxy- 102 C6H140 036839-67-5 9 4 Butane, -methoxy-2-methyl- 102 C6H140 000994-05-8 9 Abundance ! Scan 344 (8.199 min): 31587.D (-) m/z 73.00 100.00% 73

5000 43

87 103 7.80 8.00 8.20 8.40 8.60 38 I, | 50 55, . 1 1 I 1 1 1 1 1 1 1 1 • i ■ • ■ 1 I1 1 ■ , । ... i । . . . . J 67, 1 m/z 43.05 29.27% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 7)3

5000 7.80 8.00 8.20 8.40 8.60

45 m/z 41.05 11.12% 15 53 59 88 miz-> • ■ i ' r 10 20 ------------HL 30 40 50 60 I ■ ' 1 1 i 1 ' ■ ■ 1 ■ 70 1 1 ■ i 80 90 100 110 Abundance #292: N-Ethyiformamide 30 73 7.808.00 ' 8.20 ' ' 8.40 1 8.60 5000 m/z 45.05 10.83% 44 58

15 . ! .! ' I 1 1 1 1 i 1 1 1 1 I r miz-> 10 20 30 40 50 60 70 80 90 100 110 'Abundance #1793: Pentane, 3-methoxy- 7.80 8.00 8.20 8.40 8.60 m/ z 71.00 6.51%

m/z-> 5000-

i ■ ■ ■ ■ । 10 20 27 33 39. • ■ • • i ■ ■ • ■ । 30 40 । 45

55 i ' —— 1 1 ‘ 1 H I ■ ■ i ■ ■ ■ ■ । 50 60 70 80 90 ■ i ■ ■ •

100 ■ i •

110 7.80 8.00 L 8.20 8.40 8.60

31587.D GCMS0208.M Wed Feb 27 12:02:33 2002 Page 1

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