GCMS analysis results for sample AE03916, Mar 15 2002

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Data File : C:\HPCHEM\l\DATA\FEB2102\3916.D Vial: 78 Acq On : 24 Feb 2002 10:46 pm Operator: Sample : gc/ms scan 2/22 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ************************************************************ * ******** Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 4.14 ug/1 313776 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tramethyl - 88 C4H12S1 000075-76-3 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1-Butanamine , 3-methyl- 87 C5H13N 000107-85-7 9 4 Pentane, 3-methoxy-_________ ______ 102 C6H140 036839-67-5 9 Abundance 7 Scan 344 (8.198 min): 3916.D (-) m/z 73.00 100.00% 73

5000 43 । / - ii

87 7.80 8.00 8.20 8.40 8.60 38 |, | 50 5,5. 67, । 103 ■ ■ । ■ 1 I ■ ■ ■ >■ |-i-i-i-i । i । , . । . । . । । . . . . । 4 TT 1 1 m/z 43.05 29.61% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73

5000 7.80 8.00 8.20 8.40 8.60 45 m/ z 4 5.0,5 10.69% | 15 -| 1 1 1 1 I 1 TT I 1 — 53 59 ।| 88 i ■ ■' ■ T‘‘i . . . . । . I1 1 1 1 1 ' 1 1 I 1 1 । • i ' ■ ■ • i ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 'Abundance #292; N-Ethylformamide 30 73 ' I 1 ' 1 1 1 1 — 1 7.80 8.00 8.20 8.40 8.60 5000 m/z 41.05 10.41% 44 58

15 ■ J i ■ ■ ■ ■ I ' 1 1 1 I ' 1 1 ' I 1 1 1 1 I ■ ■ 1 ■ i ■ ■ ' 1 i 1 ■ ■ ' i ' ■ ' 1 I ■ ■ ■ ' i ■ ■ ' ' i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 'Abundance #763: 1-Butanamine, 3-methyl- TE—T 30 7.80 8.00 8.20 8.40 8.60 m/z 71.00 7.21% 5000

51 41 55 70 87 1 - i

,m/z--> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

3916.D GCMS0208.M Wed Mar 13 11:37:52 2002 Page 1

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