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GCMS analysis results for sample AE03916, Mar 15 2002

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Laboratory report documenting GCMS analysis of sample AE03916 conducted on March 15, 2002.

NYC-WTC_000038292–000038301

Folder label: “GCMS X 2/22/02 A 2/24/02

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Scanned page image, NYC-WTC_000038300
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB21O2\3916.D Vial: 78 Acq On : 24 Feb 2002 10:46 pm Operator: Sample : gc/ms scan 2/22 fb Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L

Peak Number 2 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.87 0.23 ug/1 23427 Phenanthrene-dl0 25.73

Hit# of 5 Tentative MW MolForm CAS# Qual

1 Phenanthrene -d10 188 C14D10 001517-22-2 80 2 Anthracene-dll)- 188 C14D10 001719-06-8 50 3 -(4-Tolyl)-/-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 38 4 3-Quinoline arbonitrile, 1,2,3,4-te 188 C10H8N2O2 022384-05-0 37

L Abundance Scan 2269 (25.870 min): 3916.D (-) m/z 188.10 100.00% I 188

i ■ 5000-

80 94 158

j m/z-> 60 ' 1 i ' S4...1. 70 80 90 100 110 120 130 140 150 4 160 170 180 190 m/z 25.60 25.80 26.00 26.20 93.95 19.66% ’Abundance #19958: Phenanthrene-d10 i 188

5000 25.60 25.80 26.00 26.20 80 m/z 189.101 16.35% 94 160 — —PP 66 |- — • — , 44 |1 m/z—> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d 10- 1 188

25.60 25.80 26.00 26.20 5000 m/z 158.05 16.01%

66 8,° TTTaTT——TT IT 94 160 ......4 m/z-> 60 70 80 90__100 110 120 130 140 150 160 170 180 190 Abundance #19863: -(4-Tolyl)-3-methyl-pyrazol-5-one ■ ■ i ■ 1 TI8 r 188 25.60 25.80 26.00 26.20

1 91 m/z 186.10 13.69% 105 5000- 119 65 78 ■ ' i ' ' ' ' i ' - — B — T - *P r— 146 ——— TII I m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

3916.D GCMS0208.M Wed Mar 13 11:37:56 2002 Page 2

NYC-WTC_000038300

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NYC-WTC_000038300Source: NYC Law Department, mirrored locally

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