GCMS analysis results for sample AE04125, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2202\4125.D Vial: 21 Acq On : 23 Mar 2002 3:46 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank I

R.T. EstConc Area Relative to ISTD R.T.

8.14 3.60 ug/1 441951 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 Silane, tramethyl- 88 C4H12Si 000075-76-3 23 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 1,3-Dicxolane, 2-methyl - 88 C4H802 000497-26-7 9 Abundance Scan 337 (8.141 min): 4125.D (-) m/ z 73.00 100.00% 73

5000 43

87 7.80 8.00 8.20 8.40 .......... , , 38.1 A 50 55 ■ ' i ■ ' ■ ■ i • ‘ ■ I ■ ■ ‘ 1 I1 67,1 103 ■ । • ■ • • । ■ ■ • • । • 1 11•' । ■ ■ ■ ■ । •' • ■ । ■ m/z 43.05 30.16% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73

5000 1*177 7.80 8.00 8.20 8.40 45 m/z 45.0.5 10.68% 15 . I 53 59 I 88 i ■ ■ i 1 ''' ' 1 ‘ ‘ ■ I ' ' ‘ ‘ I 1 ' ' ' I •'•’■’I’l .... 1 . I ■ ■ i • ■ ■ ■ i ■ ■ ■ • i ■ ■ ■ ' i ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformende 30 73 ................ /............ i 1*1***I**’ rrr* • i ‘ * * * r I 7.80 8.00 8.20 8.40 5000 m/z 41.05 10.48% 44 58 15 ' ‘ l n—r-rj-r ■ । ' ■ ■ ■ । ■ ■ ■ ■ । ■ ■ • ■ । ■ ■ ■ ■ । ■ 1 • ■ । • 11 ■ । ' 1 । ■ 1 1 1 । ' m/z-> 10 20___ 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- dm 1-daai 14* r । । । I 30 7.80 8.00 8.20 8.40 m/z 6.71% 71 • 0,0 5000

15 41 55 70 87 ■ ■ .'i'll. ■ i ■ ■ । 1 1 1 ' I 1 1 1 ' i 1 1 '' i ‘ ITT । । i । । 1m i । ' ' l ' ‘ I ‘ ' ■ i ' ■ ' ■ i ■ 1II m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

4125.D GCMS0308.M Wed Mar 27 10:01:35 2002 Page 1

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