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GCMS analysis results for sample AE12675, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12675 conducted on June 6, 2002.

NYC-WTC_000015016–000015026

Folder label: “GCMS X 5/30/02 A 6/1/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\MAY3 102\12675.D Vial: 20 Acq On 1 Jun 2002 6:41 am Operator: Morgan Sample gc/ms scan 5/30 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P 2** Quant Method : C:,\HPCHEM\1\METHODS\GCMS0531 .M (RTE Integrator) - Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 25.57 0.46 ug/1 43096 Phenanthrene-dl0 25.43 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenant hrene-d10 188 C14D10 001517-22-2 86) 2 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 42 3 Antipyrine 188 C11H12N2O 000060-80-0 33 4 Anthracene -dlO- 188 C14D10 001719-06-8 28 Abundance Scan 2236 (25.574 min): 12675.D (-) m/z 188.10 100.00% 118

5000

80 94 66 156 25.20 25.40 25.60 25.80 26.00 51 m*- TL ’’ m/z 93.95 18.21% mtz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 11)8

5000 25.20 25.40 25.60 25.80 26.00 m/z 189.10 14.71% 80 94 160 66 i ■1 ■11111 ■ i'1 ■' i11111 ■11 d ■' - " I ‘11 ‘ ‘ ■ i ■ i" mfz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69165:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 1118

25.20 25.40 25.60 25.80 26.00 5000 m/ z 80.00 14.12% 143 • 89 116 130 b 158 170 1111" 1111111111 1’L mjthpmnaans III, “ I' ‘" I ’ “ * I'1 ‘11 “ 11111111111111 1 miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69176: Antipyrine 1118 25.20 25.40 25.60 25.80 26.00 m/z 65.95 7.76% 96 5000 77 56 105 -116 “ i ■ " ■ i ■ ■ 129 159 173 Hi ■ " ' i " i “ " I " ■ ■ i “ “ i ■ ■ ■ ■ i “ ’117 IL tnfz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.20 25.40 25.60 25.80 26.00

12675.D GCMS0531.M Mon Jun 03 11:45:23 2002 Page 3

NYC-WTC_000015025

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NYC-WTC_000015025Source: NYC Law Department, mirrored locally

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