GCMS analysis results for sample AE12575, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY3102\12575.D Vial: 9 Acq On : 31 May 2002 7:51 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P 2** Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) ... Title : 20*9 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 25.57 0.45 ug/1 44163 Phenanthrene-dl0 25.43 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-dl0^188 C14D10 001517-22-2 86 ; 2 Anthracene-diO- 188 C14D10 001719-06-8 86 / 3 4H-Pyridb[l,2-a]pyrimidin-4-one, 3- 188 C11H12N2O 057773-19-0 33 4 2-Quin inecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 9 Abundance Scan 2236 (25.569 min): 12575.D (-) m/z 188.10 100.00% 188

5000

94 25.20 25.40 25.60 25.80 1,1 49 66 80 | 156 i “ “ i " ■ • i • ■1 • i ■ " 11" “ i11 ■ ■ i ■ ■ “ I “ 111 11 ■1 ■11 “ ■ ‘ i " 1111 ■ " i ■1 “ I ■ 1 m/z 9 f4.00 17.96% miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

5000 25.20 25.40 25.60 25.80 ‘‘' m/z 189.10 17.04% 80 94 160

miz—> Abundance 40 50 60 66 PPP - 70 80 m ... W. 90 100 110 120 130 140 150 160 170 180 190 #19957: Anthracene-d10- 1118 • i • • ■ * । • i ■ 25.20 25.40 25.60 25.80 5000 m/z 184.10 15.34%

m/z—> 40 Abundance s 50 60 70 80 T1'' • |11 111 " 1 111 1 “ 11 90 100 110 120 130 140 150 160 170 180 190 #19873:4H-Pyrido[1,2-alpyrimidin-4-one, 3-ethyl-6-methyl- 160

145 118 25.20 25.40 25.60 25.80 173 m/z 92.00 8.99%

5000 92 65 159 -119—12-+ । • ■ ■ • ।" ■11 ■11111"' i": 11 | mlz~> 40 50 60 70 80 90 100 T10 120 130 140 150 160 170 180 190 1 ■ i ■1 “ i ‘'

25.20 25.40 2560 25.80

12575.D GCMS0531.M Mon Jun 03 09:35:03 2002 Page 3

NYC-WTC_000014921