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← Document results/DEP Box 15/GCMS X 5/23/02 A 5/30/02
Document / 11 pages

GCMS unknowns report for sample AE12282, June 2002

Machine-extracted title · confidence 100%

Report documenting analysis for unknown compounds and surrogate recovery in sample AE12282.

NYC-WTC_000013751–000013761

Folder label: “GCMS X 5/23/02 A 5/30/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2902\12282.D Vial: 23 Acq On : 30 May 2002 8:56 am Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Phenanthrene-diO Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

25.57 0.43 ug/1 49659 Phenanthrene-dl0 25.43 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene -d10/7 188 C14D10 001517-22-2/87 2 Anthracene-diO- 7 188 C14D10 001719-06-81 83 3 Cyclohexanone, phenylhydrazone 188 C12H16N2 000946-82-7 33 4 -(4-Tolyl)-3-methyl-pyrazol -5-one 188 C11H12N2O 035496-19-6 9 Abundance Scan 2235 (25.566 min): 12282.0 (-) m/z 188.10 100.00% 1)18

5000

* 1 * • • • | ■ T ' rl • 1 • > 1 * 1 1 > ] ■ 40 54 66 80 94 160 25.20 25.40 25.60 25.80 ndoobovpoboopodbaguuddoBnap—bospua " 111 | 11'| 1111.11111 H'| 1111111 m/z 189.10 16.24% mlz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 118

5000 II**TT1---41446111 25.20 25.40 25.60 25.80 m/z 79.95 13.14% 80 94 160 *1 66 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 i ••“ i• • “ i • “ ■ i •• l Abundance #19957: Anthracene-d10- 118 *1d,////mK/—nT 25.20 25.40 25.60 25.80 5000 m/z 184.10 11.84%

66 80 94 160

m/z—> 1111'1 ‘ I' ‘1' 1'11 ‘ 11 “ ' 11 “ ■ i11 ■ ■ i ■' ’ ■ i ■ ■ “ i “ ■ ■ i ■ “ • i ■ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 H Abundance #19927: Cyclohexanone, phenylhydrazone • i •• > ■ ।.t । i । i । । i। । । i i । । 1118 25.20 25.40 25.60 25.80 93 m/z94.00 9.75% 5000 65 77 106 145 ...120 132. 159 170. I. 4||— ■ i1 ■ i■ “'i “ “ I“• "i1 ■ ■ ■ i ■ ■ ■ ■ i■ ■ • ■ i"■ • i■■ ■■ i■*• i• ■ • । ‘। •1 i f ■■ 11111 •! 11 iz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.20 25.40 25.60 25.80

12282.D GCMS0528.M Thu May 30 10:39:36 2002 Page 3

NYC-WTC_000013760

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NYC-WTC_000013760Source: NYC Law Department, mirrored locally

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